We have studied structural and superconducting properties of MgB 2 thin films doped with carbon during the hybrid physical-chemical vapor deposition process. A carbon-containing metalorganic precursor bis(methylcyclopentadienyl)magnesium was added to the carrier gas to achieve carbon doping. As the amount of carbon in the film increases, the resistivity increases, T c decreases, and the upper critical field increases dramatically as compared to clean films. The selffield J c in the carbon doped film is lower than that in the clean film, but J c remains relatively high to much higher magnetic fields, indicating stronger pinning. Structurally, the doped films are textured with columnar nano-grains and highly resistive amorphous areas at the grain boundaries. The carbon doping approach can be used to produce MgB 2 materials for high magnetic-field applications. a)Electronic address: avp11@psu.edu

The solubility of potassium clavulanate in ethanol, 1-propanol, 1-butanol, 2-propanol, and 2-methyl-1propanol between 273 K and 305 K were measured using a laser technique. This method was used to determine the dissolution of the solid phase in a solid + liquid mixture. Results of these measurements were correlated with a semiempirical equation.

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Polymorphic transformation of pravastatin sodium in a mixture of isopropanol and water was studied by use of online focused beam reflectance measurement (FBRM) and particle vision measurement (PVM). It is shown that the form A polymorph transformed to the stable polymorph, form B. It was speculated that in the transformation process there was an agglomeration and breakage phenomenon. The transformation mechanism was identified as solution-mediated phase transformation. Influences of temperature, solvent composition, and stirrer speed on the transformation process were examined. It can be seen from the FBRM monitoring results that higher temperature, larger ratio of water to isopropanol, and higher stirrer speed can increase the transformation process.