Low density and strong mechanical characteristics make hollow glass microballons (HGM) filled polyehteretherketone (PEEK) composites excellent for aerospace, transportation and civil applications. In this study, PEEK was filled with different densities of HGMs (low, medium, and high) and varied volume fractions (Vf) of HGMs (10%, 15%, and 20%) and exposed to different strain rates to investigate thermal, physical, energy absorption, and other physico-mechanical responses. PEEK/HGMs composites demonstrated a substantial strain rate impact, with the strain rate sensitivity factor increasing as the strain rate increased while decreasing as the filler Vf increased. The density of the composites was also shown to be inversely related to their strength properties. Incorporating high-density HGMs into the PEEK resulted in the lowest composite density so far reported while ensuring mechanical properties. Scanning electron microscopy images revealed that the HGM dispersion is uniform inside the matrix. Thermal stability of the syntactic foam was investigated by using Thermo Gravity Analysis (TGA) under inert atmosphere and oxidative environment conditions. The infusion of microspheres enhances the thermal stability of LDPEs, MDPEs, and HDPEs samples in an inert environment, with HDPEs samples being the most thermally stable. This might lead to the formation of a strong bond between polymer chains and HGM particles.
Nanofillers can be added to polymers to improve their mechanical behavior. However, the yield behaviour of most polymer composites is influenced by strain rate. The majority of the research focused on the behaviour of polymer composites at high strain rates. This work aims to investigate how hydroxyapatite (HAP) and reduced Graphene Oxide (rGO) nanofillers affect the mechanical properties of sulphonated polyetheretherketone (sPEEK) at low (tensile and compression behaviour) and high strain rates (compression behaviour). The thermal, mechanical, and energy absorption responses of sPEEK filled with HAP and varying mass fraction (Mf) of rGO (0.5%, 1%, and 1.5%) at different strain are studied in detail. The strong strain rate effect was seen in HAp and rGO loaded sPEEK composites. The strain rate sensitivity factor of sPEEK-HAP/rGO improved as the strain rate increased, but decreased when the Mf of rGO increased. Under low strain rate compression, HAp and rGO loaded sPEEK absorbed more energy at Mf about 4%. SEM micrography was used to study the microstructures of the fractured interfaces of the components, revealing that the HAp and sPEEK materials formed a good compatibility in presence of rGO.
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