The in-situ observation is of great significance to the study of the growth mechanism and controllability of two-dimensional transition metal dichalcogenides (TMDCs). Here, the differential reflectance spectroscopy (DRS) was performed to monitor the growth of molybdenum disulfide (MoS2) on a SiO2/Si substrate prepared by chemical vapor deposition (CVD). A home-built in-situ DRS setup was applied to monitor the growth of MoS2 in-situ. The formation and evolution of monolayer MoS2 are revealed by differential reflectance (DR) spectra. The morphology, vibration mode, absorption characteristics and thickness of monolayer MoS2 have been confirmed by optical microscopy, Raman spectroscopy, ex-situ DR spectra, and atomic force microscopy (AFM) respectively. The results demonstrated that DRS was a powerful tool for in-situ observations and has great potential for growth mechanism and controllability of TMDCs prepared by CVD. To the best of the authors’ knowledge, it was the first report in which the CVD growth of two-dimensional TMDCs has been investigated in-situ by reflectance spectroscopy.
In order to deal with the problem of composite damage location, an imaging technique based on differential signal and Lamb wave tomography was proposed. Firstly, the feasibility of the technique put forward was verified by simulation. In this process, the composite model was regularly set down by the circular sensor array, with each sensor acting as an actuator in sequence to generate Lamb waves. Apart from that, other sensors were used to collect response signals. With regard to the damage factor, it was mainly determined by the difference between the damage signal and the non-damage signal. The probabilistic imaging algorithm was employed to carry out damage location imaging. Then, experiments were carried out so as to study the selected composite plate. Finally, the tentative outcomes have illustrated that the maximum error of damage imaging position was 7.07 mm. The relative error was 1.6%. In addition, the method has the characteristics of simple calculation and high imaging efficiency. Therefore, it has large technical potential and wide applications in the damage location and damage recognition for composite material.
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