Wire arc additive manufacturing (WAAM) is an additive manufacturing process based on the arc welding process in which wire is melted by an electric arc and deposited layer by layer. Due to the cost and rate benefits over powder-based additive manufacturing technologies and other alternative heat sources such as laser and electron beams, the process is currently receiving much attention in the industrial production sector. The gas metal arc welded (GMAW) based WAAM process provides a higher deposition rate than other methods, making it suitable for additive manufacturing. The fabrication of mild steel (G3Si1), austenitic stainless steel (SS304), and a bimetallic sample of both materials were completed successfully using the GMAW based WAAM process. The microstructure characterization of the developed sample was conducted using optical and scanning electron microscopes. The interface reveals two discrete zones of mild steel and SS304 deposits without any weld defects. The hardness profile indicates a drastic increase in hardness near the interface, which is attributed to chromium migration from the SS304. The toughness of the sample was tested based on the Charpy Impact (ASTM D6110) test. The test reveals isotropy in both directions. The tensile strength of samples deposited by the WAAM technique measured slightly higher than the standard values of weld filament. The deep hole drilling (DHD) method was used to measure the residual stresses, and it was determined that the stresses are compressive in the mild steel portion and tensile in austenitic stainless steel portion, and that they vary throughout the thickness due to variation in the cooling rate at the inner and outer surfaces.
A dissimilar welded joint of Inconel 718 and 304L austenitic stainless steel was prepared using a combined procedure with the gas tungsten arc welding and shielded metal arc welding processes by employing the Ni-based fillers: ERNiCr-3 and ENiCrFe-3. The welded joints were investigated for metallographic testing and mechanical properties, and a relationship was established between the microstructure and the resultant mechanical properties. Microstructural observation revealed the formation of the unmixed zone on the 304L SS side. The weld metal showed that the fully austenitic microstructure consisted of the Nb- and Ti-rich carbide phases along the inter-dendritic spaces. The tensile test results at room temperature showed the failure from the weld metal which might be due to alloying element segregation along the inter-dendritic spaces. However, a tensile test at 600 °C showed the failure from the 304L SS base metal with a tensile strength and % elongation value of 377 MPa and 24%, respectively. The hardness plot showed the average hardness value of the weld metal of 236 ± 5 HV, which was higher than the 304L SS BM (204 ± 4 HV) but lower than the IN718 BM (243 ± 5 HV). The impact toughness of the weld metal was 109 J, which was significantly lower than the base metals. The poor impact strength of the weld metal might be due to the evolution of the NbC phase along inter-dendritic spaces.
In the present work, the creep strength-enhanced ferritic martensitic P92 steel was welded with 304L austenitic stainless steel. The dissimilar joining of these two different grades of material was performed by using tungsten inert gas welding process. The nickel-based ERNiCr-3 welding consumable was used. The influence of post-weld heat treatment (760 °C, 2h), called as tempering, was also investigated. The secondary electron and optical image confirmed that ERNiCr-3 weld metal is accompanied by an equiaxed austenitic microstructure with Ni weight percentage of 68.29%. The energy-dispersive X-ray spectroscopy and electron probe microanalyzer results of the weld fusion zone revealed the Nb, Cr, and Ti segregation in the inter-dendritic region. The elemental mapping of the carbon-depleted zone, and the interface was performed using an electron probe microanalyzer, which revealed the diffusion of Ni, Cr, and Fe across the interface of P92 steel and ERNiCr-3 filler weld. The tensile test result indicated that part of the dissimilar weld joints (DWJs) with relatively weak ultimate tensile strength was ERNiCr-3 weld metal. The ultimate tensile strength value of the DWJs was observed as 610 MPa and 580 MPa in the as-weld and post-weld heat treatment situations, respectively. The Charpy V-notch impact energy of the ERNiCr-3 weld fusion zone was achieved as 135 ± 2 J and 140 ± 2 J in as-weld and post-weld heat treatment situations, respectively. The low impact toughness of the ERNiCr-3 weld metal was attributed to the presence of niobium carbide (NbC) and titanium carbide (TiC) particles. The peak longitudinal residual stress of 490 MPa and transverse residual stress of 442 MPa were noted in the ERNiCr-3 weld fusion zone at a depth of 3 mm from the top surface. The tempering heat treatment exhibited a significant drop in the residual stresses value for the weld fusion zone and heat affected zone (HAZ).
In India, during mining and ore processing, ore fine generation is a common phenomenon, in which more than 60% of process ore becomes discarded material. To explore the alternative of high-grade ores, mutual replacement with the utility of dump ore fines is the best way. With this perspective, Kiruburu iron ore mine (Iron Ore No.1) and Meghataburu iron ore mine (Iron Ore No.2) dumped fines were chosen for a Blaine no. investigation, in the connection of firing temperatures, to get optimum desirable physical properties, Cold Compression Strength (C.C.S.),and Apparent Porosity (A.P.), with physico-chemical properties, Reducibility Degradation Index (R.D.I.), and Reducibility Index (R.I.). To characterize pellet properties with input variables, a microstructure phase study has been conducted using a scanning electron microscope (S.E.M.), energy dispersive spectroscopy (EDS), and X-ray diffraction analysis (XRD). The Iron Ore No.1 and 2 fine pellets survey showed good, desirable properties, at the Blaine no., of 1678 cm2/g and 2311 cm2/g (corresponding to 200 mesh size), and the best results are attained at a firing temperature of 1300 °C. Thermal kinetic analysis of the heating of pellets has been done to knowthe activation energy of different ore characteristics. The results showed that Iron Ore No.2 pellets have high activation energy.
The 9% Cr steels were developed for ultra-supercritical (USC) power plants to meet the requirements of high operating temperature and pressure. These steels are produced to operate at high temperatures where impact toughness is not a concern; however, it becomes important for the welded joints to have good impact toughness at room temperature for manufacturing. The present work investigates the effect of the post-weld heat treatment (PWHT) parameters, i.e., temperature and time, on the impact toughness of multi-pass gas tungsten arc welded (GTAW) joints of ferritic/martensitic grade P92 steel. The microstructural evolution in welded joints given varying post-weld temperatures and times was studied. The lath martensitic structure of the weld metal for the as-welded joints resulted in high hardness and low impact toughness. The weld fusion zone toughness was 12 J, which was lower than the minimum specified values of 41 J (ASME standards) and 47 J (EN ISO 3580:2017). The PWHT temperature and time were found to have a significant effect on the impact toughness of the weld metal. A drastic increase in the impact toughness of the weld metal was noticed, which was attributed to lath break-up, reduction in dislocation density and reduction in solid solution hardening. The maximum impact toughness of 124 J was measured for PWHT temperature and time of 760 °C and 120 min, respectively. The effect of PWHT parameters on tensile strength was also investigated, and test results showed that the joint was safe for USC boiler application as it failed from the region of the P92 base metal. The variation in microstructural evolution along the weldments resulted in hardness variation. PWHT led to homogeneity in microstructure and, ultimately, reduction in hardness value. According to the study, the optimum temperature and time for PWHT of a GTAW joint of P92 steel were found to be 760 °C and 120 min, respectively.
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