The project consists in the implementation of a biocomposite based on tannin resin and natural rubber matrices with the bast fibres of Triumfetta cordifolia A.Rich. "Okong" from the equatorial region of Cameroon as reinforcement. A study of this still little known fibre is necessary. This paper evaluates the physico-chemical and mechanical characteristics of the fibers. The fibers are extracted by us. A series of experiments is conducted for this purpose: morphological observation with a scanning electron microscope (SEM); density evaluation with a helium pycnometer; absorption rate evaluation according to the protocol available in the literature, Fourier Transform Infrared Spectrometry (FT-IR), chemical composition evaluation according to ASTM 1972 and ASTM 1977 standards, thermogravimetric analysis (TGA) and tensile tests on fiber bundles according to NF T25-501-3. The results show that the fiber is made up of several elementary fibers with oval cross-sections. A density of 1.477 g/cm 3 close to that of hemp. These fibers have a water absorption rate of 342.5%, which correlates with the presence of free hydroxyl functional groups obtained from the spectrometry study (FT-IR). Chemical analysis reveals that the fiber is made up of celluloses (44.4%), hemicelluloses (30.8%), lignins (18.9%), pectins (3.3%), waxes (0.5%) and minerals (2.1%). In addition, we learn that the fibers studied dehydrate at 11.49%, showing a notable thermal stability around 235˚C with a peak thermal decomposition of
Fine hemp fibers (cottonized hemp) were processed using steam explosion. The quantification of the defibration rate was performed by image processing. Based on this method, the hemp defibration was optimized using a response surface methodology based on three-variable central composite design for the production of elementary fibers with low variability. Optimal parameters for the steam processes were as follows: time = 4.1 min; temperature = 191℃. Biomass was impregnated with a solution of NaOH (8%) before treatment, leading to a defibration rate of 91.2%, which is producing ≈50% fibers with length <3 mm, in good agreement with the experimental data. Damaged fibers originating from the conjugated effect of steam explosion and alkali hydrolysis were also observed.
Chestnut hydrolysable tannins are phenolic materials that have been considered too unreactive to compete in the phenolic resin adhesives market for exterior boards for the building industry. However, an article in 1973 describing 3 years industrial application of chestnut hydrolysable tannins during the first oil crisis indicated that this was not the case. We have extended this old work by using superior phenolic resins formulations and producing phenol-formaldehyde-chestnut tannin adhesives where a substitution of up to 80% of the phenol is possible with remarkably good results. The reactions involved were clarified by 13C NMR and MALDI-TOF mass spectrometry
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