Low ice adhesion surfaces are a promising anti-icing strategy. However, reported ice adhesion strengths cannot be directly compared between research groups. This study compares results obtained from testing the ice adhesion strength on the same surface at two different laboratories, testing two different types of ice with different ice adhesion test methods at temperatures of -10 o C and -18 o C. One laboratory uses the centrifuge adhesion test and tests precipitation ice and bulk water ice, while the other laboratory uses a vertical shear test and tests only bulk water ice. The surfaces tested were bare aluminum and a commercial icephobic coating, with all samples prepared in the same manner. The results showed comparability in the general trends, surprisingly, with the greatest differences for bare aluminum surfaces at temperature -10 o C. For bulk water ice, the vertical shear test resulted in systematically higher ice adhesion strength than the centrifugal adhesion test. The standard deviation depends on the surface type and seems to scale with the absolute value of the ice adhesion strength. The experiments capture the overall trends in which the ice adhesion strength surprisingly decreases from -10 o C to -18 o C for aluminum and is almost independent of temperature for a commercial icephobic coating. In addition, the study captures similar trends in the effect of ice type on ice adhesion strength as previously reported and substantiates that ice formation is a key parameter for ice adhesion mechanisms.
To lower the ice adhesion strength is the most efficient technique for passive ice removal for several applications. In this paper, the effect of different types of ice on the ice adhesion strength was investigated. The ice types precipitation ice, in-cloud ice and bulk water ice on the same aluminum substrate and under similar environmental conditions were investigated. The ice adhesion strength was measured with a centrifugal adhesion test and varied from 0.78 ± 0.10 MPa for precipitation ice, 0.53 ± 0.12 MPa for in-cloud ice to 0.28 ± 0.08 MPa for bulk water ice. The results indicate that the ice adhesion strength inversely correlates with the density of ice. The results inspire a new strategy in icephobic surface development, specifically tailored to the relevant ice type.
In order to develop an effective deicing device using mechanical deformation of substrates, the adhesive and/or cohesive strains of ice at rupture were measured for three different modes of solicitation: tensile, twisting and bending. A total of 108 icing/deicing tests were conducted with aluminum and nylon samples covered with hard rime ice deposits 2, 5, and 10 mm thick strained at various strains rates in brittle regime at −10°C. Real time deformation was precisely monitored using a strain gage fixed to the A1 interface, and force by means of load cells and a torque-meter. Deicing strain was determined at the time of ice detachment, which corresponds to a visible, instant change in the slope of stress-strain curves. The mean values of deicing strains, ε %, measured in tensile, torsion and bending experiments are respectively, 0.037 ± 0.015%, 0.043 ± 0.023% and 0.004 ± 0.003% As for adhesion strength, the highest values were obtained in tension, 4 MPa ± 50%, and the lowest in bending, 0.014 MPa ± 36%. In torsion, the value was intermediary, at 1.26 MPa ± 67%. Measurements also showed that deicing stress and strain tended to increase with substrate roughness, whereas they decrease with increasing ice thicknesses. In summary, this work points out the effects of two major factors on ice adhesion strength, the solicitation mode and the ice thickness. Finally these results suggest that the first criteria for a mechanical deicing device has to satisfy to be effective is to have the capacity to generating a strain at around 0.04% ice/substrate interface.
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