Outstation, Hamburg, FRG) for measuring the EXAFS spectra.Registry No. [L4Fe4(M-0)2(M-OH)4]I4-3H20, 123567-48-6; [L4Fe4-(µ-0)2(µ-0 )4]( 04)4•3 20, 123567-50-0; [L2Fe2(acac)2^-0)]-(C104)2, 118486-84-3; LFeClj, 86823-88-3. Supplementary Material Available; Tables of complete crystallographic data, bond distances and angles, and thermal parameters (5 pages); a listing of structure factor amplitudes (43 pages). Ordering information is given on any current masthead page.
The newly synthesized Mo(VI) complexes (I) with sterically bulky ligands undergo one electron reversible electrochemical reduction to give Mo(V) monomers.
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