Summary
The use of agro‐industrial waste for food enrichment can be limited, due to taste, odour, colour and other unpleasant characteristics. Trub (brewing waste) has important nutrients, such as proteins and carbohydrates, and phytochemical compounds; however, its applications are hindered by the astringent flavour. In order to reduce the bitterness of trub, aqueous extractions were realized at high temperature (100 °C per 1 h) in five steps. Two fractions were obtained; a liquid fraction (containing bitter compounds) and a solid fraction (the trub after the extraction process; TAP). Both fractions and the trub before the extraction process (TBP) were evaluated. The bitterness of TBP was significantly reduced in TAP while the protein content increased; TAP presented a branched network and changes in its structure. The reduction in bitterness and the high protein content allows the use of trub in the food industry.
The recovery of bioactive compounds from agro-industrial residues with green solvents in ultrasound-assisted extraction (UAE) processes represents an interesting alternative from environmental and economical perspectives. Here we investigated optimal conditions to improve the extraction of anthocyanins from blackberry pomace. The experimental data were fitted to the second-order polynomial model to obtain the regression coefficients, and three-dimensional (3-D) response surface plots were considered to represent the relationships between each variable on the response of total monomeric anthocyanin (TMA) content. The ultrasound-assisted process at an ultrasound amplitude of 40% for 10 min and a concentration of 25 mg/L resulted in the maximum TMA concentration of 1.39 ± 0.02 mg Cy3GlE /g. At these extraction conditions, the extract presented total polyphenol and flavonoid contents of 44.12 ± 0.17 mg GAE /g and 63.25 ± 0.53 mg QE /g, respectively. A total of 31 individual compounds, including anthocyanins, flavonols, and phenolic acids, were identified in the extract. Concentrations of cyanidin-3-glucoside and caffeic, gallic, and ellagic acids were 2.38 ± 0.09, 0.47 ± 0.01, 0.55 ± 0.01, and 0.48 ± 0.01 mg/g, respectively. Compared to the conventional extraction, the UAE represented an increase of 20.87% in total anthocyanins. Thus, the UAE at suitable conditions is suggested to recover bioactive compounds from blackberry pomace.
Practical ApplicationsThe use of blackberry pomace to extract bioactive compounds is promising because it uses a by-product from the fruit processing industry. This study presents an innovative proposal of optimal process conditions to recover anthocyanins from blackberry pomace under ultrasound irradiation. The use of green solvents, as water, in ultrasound-assisted extraction (UAE) processes, represents an interesting alternative from environmental and economical perspectives, UAE process is a favorable, fast, efficient, and environmentally friendly method. The obtained blackberry pomace powder is an interesting ingredient to food and pharmaceutical industries, mainly due to the elevated concentration of added-value compounds. Besides the high amount
The objective was to evaluate the extract stability of hibiscus in different conditions and the food application. Anthocyanins (TA), phenolic compounds (TP) and color, at: 4 and 25 °C, presence or absence of light, pH stability and FTIR were evaluated. Gelatin developed with hibiscus extract was submitted to sensory analysis. Light and temperature factors affected the stability of TP and TA throughout the storage. Higher stability was observed at 4 ºC and absence of light (in relation to TA and TP respectively, 3% and 26% losses were observed in this condition against 43% and 39% at 25 °C with light). Regarding pH, it was observed that pH change affected the absorbance and color in the hibiscus extract. Finally, the hibiscus extract, when added at the highest concentration into gelatin, was the most accepted by tastes, and scored 7 (like moderately) for color and global acceptance.
Canistel (Pouteria campechiana (Kunth) Baehni) is a tropical fruit with a yellow pulp due to the presence of carotenoids, which may be interesting for application by the food industry. The aim of this research was to analyze the phytochemical and technological characteristic of dehydrated canistel pulp by thermal dehydration and freeze-drying techniques. Test for antioxidant activities (DPPH and ABTS radical scavenging; ferric reducing antioxidant power - FRAP), total polyphenols, flavonoids, carotenoids content (UV-Vis, FTIR and Raman spectroscopy), color, and hygroscopic properties were performed. The freeze-dried sample showed a higher carotenoids concentration, more intense coloring and better hydration properties than the thermally dehydrated sample. Functional groups such as water, carotenoids, primary and secondary amides, aldehydes groups, phenolic acids, aromatic rings, cellulose, polysaccharides and niacin were identified by FTIR in both samples. Ingredient obtained by freeze drying showed better technological characteristics, allowing its use by the food industry.
Maytenus ilicifolia Mart. Ex Reissek, was first studied in the 60s, but only in the 80s and 90s were the studies were driven by scientific research that attributed medicinal properties to the plant, such as healing actions for human gastric diseases. In this work, a study was carried out on the characterization of the chemical composition of M. ilicifolia at different stages of development, using spectroscopic techniques of sustainable character, which do not require toxic solvents as previous preparations. Extracts from cotyledons, seedlings that have never been researched in the literature and leaf/stem were lyophilized to characterize the compounds present in this plant using photoacoustic and spectroscopy techniques in the Infrared spectroscopy using Fourier Transform-FTIR with ATR. The photoacoustic results show that there is a differentiation of development stages in the plant due to the greater presence of chlorophylls and terpenes in the seedlings and their absence in the cotyledon, which is characterized as the reserve part in the germination phase of the plant. The range of bands the literature reports for epigallocatechin and friedelin, the possible agents responsible for the medicinal effects of the plant were mainly seen in the cotyledon, thus demonstrating the use of the seedling in its initial stage, to extract and obtain these active components.
scite is a Brooklyn-based organization that helps researchers better discover and understand research articles through Smart Citations–citations that display the context of the citation and describe whether the article provides supporting or contrasting evidence. scite is used by students and researchers from around the world and is funded in part by the National Science Foundation and the National Institute on Drug Abuse of the National Institutes of Health.