Surface gratings associated with holographic volume gratings in photorefractive crystals of iron-doped lithium niobate have been studied using diffraction of a reflected probe beam and high-resolution phase-shifted interferometric profilometry. Both techniques show that the surface gratings exist in the form of periodical corrugations of the same period as that of the volume grating. The maximum amplitude of the periodical surface relief measured by both techniques is close to 6.5 nm. We also demonstrated that the periodical electric forces on the surface were capable of assembling polystyrene microspheres along the fringes of the grating. Large amplitude of the periodic electric field (1.6×104 V/cm) is associated with the photogalvanic effect.
We measured the reflectivity of nanoparticle thin films with bimodal size distributions clearly separated by depth and found distinctive spectral differences depending on the direction of illumination. In contrast with previous experiments that implied such differences, the samples in this experiment are prepared by ion implantation at sufficiently high energy to achieve the necessary spatial separation between larger and smaller nanoparticles. We demonstrate that the difference between scattering and absorption probabilities as a function of nanoparticle size is responsible for the differences in maximum reflectivities as the direction of illumination is reversed. This conjecture is supported by a Mie scattering calculation.
Thermoelectric generators convert heat to electricity. Effective thermoelectric materials and devices have a low thermal conductivity and a high electrical conductivity. The performance of thermoelectric materials and devices is shown by a dimensionless figure of merit, ZT = S2σT/K, where S is the Seebeck coefficient, σ is the electrical conductivity, T is the absolute temperature, and K is the thermal conductivity. We have prepared 100 alternating layers of SiO2/SiO2+ Ge superlattice thin films using ion beam–assisted deposition for the thermoelectric generator device application. The 5 MeV Si ion bombardments were performed using the Center for Irradiation Materials’ Pelletron ion beam accelerator to form quantum dots and/or quantum clusters in the multinanolayer superlattice thin films to decrease the cross-plane thermal conductivity and increase the cross-plane Seebeck coefficient and cross-plane electrical conductivity. The thermoelectric and transport properties have been characterized for SiO2/SiO2+ Ge superlattice thin films.
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