During the past eleven years (1925-35) several equilibrium diagrams involving iron as one of the components have been investigated at the National Physical Laboratory. The provision of the numerous alloys required for these researches has necessitated the production of quantities of high purity iron. Tritton and Hanson, when they began work on the iron-oxygen system at the National physical Laboratory, considered that the best commercial iron then obtainable was unsuitable for their work, and in the period 1922-24 prepared iron electronically according to the method of Cain, Schram, and Cleaves. At first the present authors produced iron in a somewhat similar manner, but when improvements in analytical methods revealed impurities in samples originally considered satisfactory, alterations were made in the method of preparation. Comprehensive analyses indicate that the latent batch of iron prepared the authors is very low in impurities, yet the physical properties of this material suggest that some disturbing factor may still be present. The problem is apparently complex and a rapid solution appears unlikely In these circumstances it was thought that the present publication of data concerning several batches of iron prepared at the National Physical Laboratory would serve a useful purpose. In addition to information obtained by the authors, particulars of a batch of iron prepared by Mr. W. E. Prytherch, M. Sc., also of the Metallurgy Department, N. P. L., are included, together with occasional results obtained by older members of tde staff. The results of Tritton and Hanson (
loc. cit
.) are omitted, how-ever, as these have already been published.
The accompanying report deals with the nature of the failure at high temperatures of certain alloy steels, which are being used to replace carbon steels, and indicates the conditions of use under which the development of intercrystalline cracking can be avoided. Investigations are being continued with a view to finding steels of high creep strength, in which the onset of intercrystalline cracking can be displaced to higher temperatures.
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