Highly efficient separation, recovery and recycling of the fluorous-tagged catalyst, [Ni[F13C6C(O)CHC(O)C6F13]2], can be achieved with fluorous solid-phase extraction, after the Lewis acid catalysed synthesis of enaminodiones in conventional organic solvents.
Separation and purification methodsSeparation and purification methods V 0200 Separation, Recovery and Recycling of a Fluorous-Tagged Nickel Catalyst Using Fluorous Solid-Phase Extraction. -(CROXTALL, B.; HOPE, E. G.; STUART*, A. M.; Chem. Commun. (Cambridge) 2003, 19, 2430-2431; Dep. Chem., Univ. Leicester, Leicester LE1 7RH, UK; Eng.) -M. Paetzel 03-236
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