Field experiments were conducted at three different sites in Saskatchewan, Canada (Colonsay, Vanscoy and Rosthern) over two years (2005 and 2006) to determine the effects of dribble-banded and coulter-injected liquid fertilizer applied in the spring of 2005 at 56, 112 and 224 kg N ha )1 with and without P at 28 kg P 2 O 5 ha )1 . The three sites were unfertilized, 7-to 8-year old stands of mainly meadow bromegrass (Bromus riparius)-dominated haylands. All fertilization treatments produced significantly (P £ 0AE05) higher dry matter yield than the control in the year of application at the three Saskatchewan sites. There was no significant difference between the two application methods (surface dribble band vs. coulter injected) for any fertilizer treatments. The addition of 28 kg P 2 O 5 ha )1 P fertilizer along with the N fertilizer did not have a significant effect on yield in most cases. In the year of application, increasing N rates above 56 kg N ha )1 did not significantly increase yield over the 56 kg N ha )1 rate in most cases, but did increase N concentration, N uptake and protein concentration. A significant residual effect was found in the high N-rate treatments in 2006, with significantly higher yield and N uptake. In 2005, the forage N and P uptake in the fertilized treatments were significantly higher than the control in all cases. The N uptake at the three Saskatchewan sites increased with increasing N rate up to the high rate of 224 kg N ha )1 , although the percent recovery of applied N decreased with increasing rate. The P fertilization with 28 kg P 2 O 5 ha )1 also increased P uptake. Overall, rates of fertilizer of approximately 56 kg N ha )1 appear to be sufficient to produce nearly maximum forage yield and protein concentration of the grass in the year of application.
CRM (Certified Reference Material) BAM-U116/CGL306 "Cyanide in soil" was produced within a framework of cooperation between CGL (Central Geological Laboratory) of Mongolia and Federal Institute for Materials Research and Testing (BAM) of Germany in 2013-2017. The CRM BAM-U116/CGL306 represents a mixture of a sandy soil collected from a contaminated former gasworks area in the Berlin region (Germany) and an unpolluted sandy soil from Nalaikh region (Mongolia). The bulk candidate material for this reference material was prepared at CGL CRM Laboratory exclusively destined to the preparation of reference materials and equipped with modern technical equipment. Homogeneity, stability and shelf life were studied in full compliance with ISO Guide 35. The CRM was evaluated as sufficiently homogeneous. Statistical evaluation of certification analysis was software packages SoftCRM and ProLab Plus. Certified value of total cyanide of the CRM is 12.0 mg/kg and expanded uncertainty was assigned as 0.8 mg/kg. The intended purpose of this material is the verification of analytical results obtained for the mass fraction of total cyanide in soils and soil-like materials applying the standardized procedure ISO 11262:2011. As any reference material, it can also be used for routine performance checks (quality control charts) or validation studies.
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