X-Ray fluorescence (XRF) is an effective method for chemical profile analysis of various materials. In earlier times, it is only confined to qualitative and quantitative analysis. This wavelength dispersive X Ray fluorescence (WDXRF) will be used to check the nuclear design of different Molybdenum compounds. The study of relative intensity ratios of various satellite peaks of Molybdenum (Mo) and Molybdenum trioxide (MoO3) compounds is associated with their atomic spectral structures. The intensity ratios will give the validity of the Hatree-slater model of different combinations. In this paper, we will present energy versus intensity and data obtained using WDXRF for the compounds Mo and MoO3. From this data, it will be seen that the Lβ line is resolved. From this we conclude that Coaster-Kronig transitions by double vacancy states of L3N4 and L3N5.
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