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In recent years, MgO-ZrO 2 composite material plays a significant role in dielectric properties for the use of capacitors and it has been considered as alternative to the conventionally used SiO 2 due to its advantages in ceramic applications. Under consideration, a series of Dy 3+ ions doped MgO-ZrO 2 have been synthesised by solution combustion method and dielectric measurements were carried out. Further, their crystal structures and optical properties were analysed and observed a notable effect. Additionally, all dysprosium doped MgO-ZrO 2 composite materials were subjected to measure electrical resistivity and found significant dielectric constants.