Fifty-four sediment samples of the five Northern Egyptian lakes, (Mariout, Edku, El-Burullus, El-Manzallah, and ElBardaweel) were analyzed to investigate the pollution status of mercury (Hg). The total mercury (T-Hg) content in sediment samples ranged from 15.33 to 171.29 ng·g -1 dry wt). The results showed that T-Hg were lower than the back ground values reported and also lower than the ranges of uncontaminated sediments. Moreover, the T-Hg concentrations in all sediments were under the upper chemical Exceedance level (1 µg·g -1 ). The concentrations of Methyl mercury (MeHg) in surface sediments of the Northern lakes ranged from 0.002 -0.023 ng·g -1 dry wt. The contribution of MeHg was less than 0.1% of total mercury concentration with index values from 0.08 -1.37 ng·g -1 ; dry wt). MeHg showed insignificant correlation with T-Hg. This suggested that MeHg contents were not controlled by the T-Hg in sediments. The T-Hg and MeHg concentrations were insignificantly correlated with TOC content which indicates that the concentration of T-Hg and MeHg in sediments of Northern lakes were not influence by TOC. The average T-Hg concentration was found in the following order; Mariout > El-Manzallah > El-Burullus > Edku > El-Bardaweel. While the MeHg was found in the order; El-Bardaweel > El-Burullus ≥ El-Manzallah > Mariout > Edku.
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