Studies were conducted to analyze the presence of 11 pesticide residues in 12 surface waters in the Piedmont and coastal plain regions of North Carolina. Samples were assayed using enzyme-linked immunosorbent assays (ELISAs). All ELISA results of one part per billion (ppb, pgfL) or greater were confirmed using gas chromatography/mass spectrometry (GCIMS). ELISA detection limits were approximately an order of magnitude higher than GCJMS methods. Of the 5,035 analytical results from 742 surface water samples, atrazine was detected in approximately 45 percent of the samples, five of which were at or above the Maximum Contaminant Level (MCL) of 3-ppb. Metolachlor was detected in 64 percent of the samples. Aldicarb, 2,4-D, chlorpyrifos, and chlorothalonil were also detected, and each was found in less than 12 percent of the samples. The remaining pesticides, including carbaryl, acetochior, methomyl, carbofuran, and alachlor, were not detected during the study period. (KEY TERMS: water quality; herbicides; North Carolina; surface water; ELISA; GCIMS) iPaper No.
Studies were conducted to analyze the presence of 11 selected pesticides in 12 surface water supply intakes in the Piedmont and coastal plain regions of North Carolina. Samples were assayed using enzyme linked immunosorbent assays (ELISAs). Samples with pesticide detection of 1 ig/L or greater were extracted and confirmed using gas chromatography/mass spectrometry (GCIMS). Detection limits of the immunosorbent assays for pesticide residues were generally an order of magnitude higher than GC1MS. Atrazine was detected in approximately 45 percent of the samples, and on two occasions was at or above the lifetime Maximum Contaminant Level of 3.0 pg/L set by the Environmental Protection Agency for an annual average in finished drinking water. Metolachlor was detected in 58 percent of the samples. Of the remaining nine pesticides, including carbaryl, aldicarb, 2,4-D, chiorpyrifos, acetochlor, methomyl, carbofuran, alachlor, and chlorothalonil, only aldicarb, 2,4-D, and chlorpyrifos were detected in less than 9 percent of the samples for each pesticide.(KEY TERMS: water quality; pesticides; drinking water; surface water; runoff; enzyme linked immunosorbent assays (ELISA).) 'Paper No.
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