The present manuscript describes a simple, sensitive, accurate, precise and economical visible spectrophotometric method for the estimation of azithromycin from tablet formulation. The method is based on the reduction of potassium permanganate in alkaline medium with azithromycin. The measurement of decrease in absorbance of potassium permanganate at 547 nm was done, as it decolourises upon reduction by azithromycin. The method was used to determine between 2 and 20 μg/ml of azithromycin in the final measured solution. There is no interference from the ingredients commonly found in azithromycin tablets with this method. The results for the determination of azithromycin in tablets were in good agreement with the labelled quantities and related analytical parameters are calculated.
Nonequilibrium molecular dynamics (MD) simulations have been performed to understand the evaporation of a liquid droplet in the presence of a solid nanoparticle. The influence of solid–liquid interaction strength (εsl) on the evaporation properties was addressed. The system consists of a solid nanoparticle (platinum) engulfed in a droplet (argon) in Argon vapor environment. After the equilibration of this nanoparticle embedded droplet with its vapor, the boundary of this system is heated continuously to evaporate the droplet. It is observed that the addition of a nanoparticle to the droplet resulted in a slower evaporation rate when compared to that of a pure droplet. It was found that the evaporation rate of the droplet is decreased with increasing solid–liquid interaction strength (εsl) and those liquid atoms around the solid nanoparticle with higher εsl are able to delay evaporation even at higher temperature owing to its decreased interfacial resistance. In order to analyze further on the vibrational coupling of the solid and liquid atoms, the vibrational density of states (VDOS) of the solid atoms is studied. It is observed that the DOS of the solid atoms exhibited a higher population in the lower frequency range with the highest peak observed for a lower value of εsl. For low values of εsl, we observe a decrease in the overlap between the VDOS of the solid atom and the interfacial liquid atoms. It is observed that for higher values of εsl, the particle is able to retain a structured layer of liquid even at high temperature and also a higher heat input is necessitated to break the interaction strength of the liquid molecules around the solid nanoparticle, which makes it possible in delaying the complete evaporation of the droplet.
This paper presents the enhancement of power quality for a microgrid system at distribution level using Shunt active power filter. The main objective of this paper is to identify a suitable pulse generation technique for obtaining a better compensation capability of shunt active power filter. The compensation capability of the device is mainly depends on the regulation of DC link capacitor voltage. Conventionally fixed hysteresis current control technique has been used. To raise the performance of shunt active power filter, an adaptive hysteresis current control technique has been proposed here. The performance of proposed technique has been verified for different operating condition in the platform of MA TLAB/SIMULINK model.
A new leaf blight disease of browntop millet (Brachiaria ramosa) was noticed during rainy season (Kharif) 2018 at small millet experimental field, University of Agricultural Sciences, Gandhi Krishi Vignana Kendra (GKVK), Bengaluru, India. To assess the disease severity, an intensive roving survey was conducted during the 2019 cropping season. Based on the morphological characterization, the causal agent of leaf blight disease was identified as Bipolaris spp. Further sequencing and combined gene analysis of ITS (internal transcribed spacer of rDNA), GAPDH (glyceraldehyde 3‐phosphate dehydrogenase) and LSU (large subunit) of all the nine isolates confirmed the pathogen as B. setariae. Pathogenicity study showed that all the isolates were pathogenic and caused leaf blight symptoms on browntop millet. The B. setariae isolates showed marked variability with respect to disease incidence on browntop millet (cv. Dundu korale) under artificial inoculation conditions. However, the host range was limited only to browntop millet and found non‐pathogenic to other six small millets examined. To our knowledge, this is the first completely described study on characterization of B. setariae causing leaf blight disease of browntop millet in India.
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