This paper presents the synergy of the effect of two surface engineering technologies—magnetron sputtering (MS-PVD) and atomic layer deposition (ALD) on the structure and properties of 316L steel. Recent studies indicate that PVD coatings, despite their thickness of a few micrometers, have many discontinuities and structural defects, which may lead to pitting corrosion after time. Applying an ALD layer to a PVD coating seals its structure and contributes to extending the service life of the coating. Investigations of the structure and morphology of the produced layers were carried out using a scanning electron microscope (SEM) and atomic force microscope (AFM). In addition, the structure of the coatings was investigated on the cross-section using a scanning-transmission electron microscope S/TEM. The tribological properties of the materials studied were determined by the ball-on-disc method. The corrosion resistance of the tested materials was determined by the electrochemical potentiodynamic method by recording the polarization curves of the anodes. Additional information about the electrochemical properties of the tested samples, including the quality, their tightness, and their resistivity, was obtained by electrochemical impedance spectroscopy (EIS). In addition, the main mechanisms of corrosion and tribological wear were determined by SEM observations after corrosion tests and after tribological tests. The study showed that the fabrication of hybrid layers by MS-PVD and ALD techniques allows obtaining coatings with electrochemical properties superior to those of layers fabricated by only one method.
The main objective of this article is to familiarize readers with the first outputs from PhD research by David Bricín, especially with the metallographic analysis, which was carried out on the first series of printed samples. The PhD thesis deals with the processing of powder mixtures based on WC-Co using selective laser melting (SLM) and other technologies. This article specifically deals with the use of SLM for the processing of a WC-Co powder mix. The grains of this powder mixture are not granular, but separate grains of carbides and binders. This powder blend was processed on a 3D SLM printer using various printing parameters. Variable parameters included laser power and scanning speed. Other print parameters were kept constant. The properties of the powder mixture and the printed samples were evaluated by metallographic analysis using light and scanning electron microscopy. These analyses were further supplemented by X-ray diffraction phase analysis, chemical analysis by EDX, and analysis of mechanical properties by compression strength testing. The evaluation of the analyses determined how the printing parameters and the type of powder used affect the development and distribution of the structure in the printed samples and how the mechanical properties of the print are then affected. For example, it has been found that increasing the scanning speed results in a more pronounced mixing between the carbide grains and the binder, which then has a positive influence on the mechanical properties of the print. In addition, the experiments found the energy at which the porosity in the printed samples was significantly reduced, and the direction in which further experiments are to take.
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