The semi organic nonlinear optical single crystal of L- Threonine Cadmium acetate Monohydrate (LTCAM) doped Ni 2+ion is prepared by the technique slow evaporation solution growth. The prepared crystal was analysed by XRD, EDAX, UV-Vis- NIR, IR, TG/DTA, Photo Luminescence (PL), VSM and SHG measurements. The SXRD shows the crystal come under the monoclinic crystal system with P21 noncentrosymmetric space group. In the visible and near infrared region the crystal shows good optical response and it is a thermally stable compound. The band gap of the grown crystal was 5.02ev. The functional groups are confirmed by FTIR analysis. The luminescent behaviour of the doped crystal shows its ability as UV filters. The dopant turns its magnetic property in to semi paramagnetic nature.
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