The 21st century and industry revolution 4.0 has been technology used part of life. This research intended to understand the effect of android application for chemistry learning (reaction rate material) to construction of motivation and metacognition of high school students. Research aimed to determine the worthiness and effectiveness of chemistry learning using android with Research and Development (R&D) method of 4D by Thiagarajan and experiment method. The instruments used in this research consist of experts' validation sheets, chemistry teachers sheets, peer reviewer sheets and students response sheets, and also test with metacognition indicators. The data were analyzed by using descriptive quantitative method with empirical analysis and MANOVA, involving two experts on topic material and media aspects, chemistry teachers and peer reviewer: the results show that on worthy grade. The result on the questions test metacognition ability and motivation sheets of trial analysis test was fit and valid questions. Therefore, the response sheets the students using android media for chemistry learning had a great influence on transfer chemistry material content of high school students. The application android was significantly effective for students metacognition ability on effect-size interpreted as large effect, but in students study motivation was not significantly effective on effect size as small effect.
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