This work investigates the use of iron oxide (III)–therminol 66 oil-based nanosuspensions in a convective heating system with potential heating applications in the buildings sector. In an experimental study, characteristics of nanofluids were measured, including heat capacity, thermal conductivity, and density. The influences of mass flow rate and concentration of nanofluid on various parameters were quantified, such as pressure loss, friction coefficient, and heat transfer rate. For a concentration of 0.3 wt.%, the heat transfer increased by 46.3% and the pressure drop increased by 37.5%. The latter is due to the higher friction and viscosity of the bulk of the nanofluid. Although the pressure drop is higher, the thermo-hydraulic efficiency still increased by 19%. As a result, iron oxide (III)–therminol 66 presented reasonable thermal performance, higher heat transfer coefficient, and a lower pressure drop value (19% better performance in comparison with water) for the air–liquid convective system. Results also showed that for nanosuspensions at 0.3 wt.%, the friction factor of the system increased by 10% in comparison with the performance of the system with water.
A detailed study was carried out to gain a better understanding of the microstructural differences between Ti-6Al-4V parts fabricated via the conventional powder metallurgy (PM) and the laser powder bed fusion (L-PBF) 3D printing routes. The parts were compared in terms of the constituent phases in the microstructure and their effects on the micro- and nano-hardness. In L-PBF parts, the microstructure has a single phase of martensitic α′ with hcp crystal structure and acicular laths morphology, transformed from prior parent phase β formed upon solidification of the melt pool. However, for the sintered parts via powder metallurgy, two phases of α and β are noticeable and the microstructure is composed of α grains and α + β Lamellae. The microhardness of L-PBF processed Ti-6Al-4V samples is remarkably higher than that of the PM samples but, surprisingly, the nano-hardness of the bulk martensitic phase α′ (6.3 GPa) is almost the same as α (i.e., 6.2 GPa) in PM samples. This confirms the rapid cooling of the β phase does not have any effect on the hardening of the bulk martensitic hcp α′. The high microhardness of L-PBF parts is due to the fine lath morphology of α′, with a large concentration of low angle boundaries of α′. Furthermore, it is revealed that for the α phase in PM samples, a higher level of vanadium concentration lowers the nano-hardness of the α phase. In addition, as expected, the compacting pressure and sintering temperature during the PM process led to variations in the porosity level as well as the microstructural morphology of the fabricated specimens, which will in turn have a significant effect on the mechanical properties.
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