The digitization of materials is the prerequisite for accelerating product development. However, technologically, this is only beneficial when reliability is maintained. This requires comprehension of the microstructure-driven fatigue damage mechanisms across scales. A substantial fraction of the lifetime for high performance materials is attributed to surface damage accumulation at the microstructural scale (e.g., extrusions and micro crack formation). Although, its modeling is impeded by a lack of comprehensive understanding of the related mechanisms. This makes statistical validation at the same scale by micromechanical experimentation a fundamental requirement. Hence, a large quantity of processed experimental data, which can only be acquired by automated experiments and data analyses, is crucial. Surface damage evolution is often accessed by imaging and subsequent image post-processing. In this work, we evaluated deep learning (DL) methodologies for semantic segmentation and different image processing approaches for quantitative slip trace characterization. Due to limited annotated data, a U-Net architecture was utilized. Three data sets of damage locations observed in scanning electron microscope (SEM) images of ferritic steel, martensitic steel and copper specimens were prepared. In order to allow the developed models to cope with material-specific damage morphology and imaging-induced variance, a customized augmentation pipeline for the input images was developed. Material domain generalizability of ferritic steel and conjunct material trained models were tested successfully. Multiple image processing routines to detect slip trace orientation (STO) from the DL segmented extrusion areas were implemented and assessed. In conclusion, generalization to multiple materials has been achieved for the DL methodology, suggesting that extending it well beyond fatigue damage is feasible.
Automated, reliable, and objective microstructure inference from micrographs is essential for a comprehensive understanding of process-microstructure-property relations and tailored materials development. However, such inference, with the increasing complexity of microstructures, requires advanced segmentation methodologies. While deep learning offers new opportunities, an intuition about the required data quality/quantity and a methodological guideline for microstructure quantification is still missing. This, along with deep learning’s seemingly intransparent decision-making process, hampers its breakthrough in this field. We apply a multidisciplinary deep learning approach, devoting equal attention to specimen preparation and imaging, and train distinct U-Net architectures with 30–50 micrographs of different imaging modalities and electron backscatter diffraction-informed annotations. On the challenging task of lath-bainite segmentation in complex-phase steel, we achieve accuracies of 90% rivaling expert segmentations. Further, we discuss the impact of image context, pre-training with domain-extrinsic data, and data augmentation. Network visualization techniques demonstrate plausible model decisions based on grain boundary morphology.
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