The double‐crystal ultra‐small‐angle neutron scattering (USANS) diffractometer KOOKABURRA at ANSTO was made available for user experiments in 2014. KOOKABURRA allows the characterization of microstructures covering length scales in the range of 0.1–10 µm. Use of the first‐ and second‐order reflections coming off a doubly curved highly oriented mosaic pyrolytic graphite premonochromator at a fixed Bragg angle, in conjunction with two interchangeable pairs of Si(111) and Si(311) quintuple‐reflection channel‐cut crystals, permits operation of the instrument at two individual wavelengths, 4.74 and 2.37 Å. This unique feature among reactor‐based USANS instruments allows optimal accommodation of a broad range of samples, both weakly and strongly scattering, in one sample setup. The versatility and capabilities of KOOKABURRA have already resulted in a number of research papers, clearly demonstrating that this instrument has a major impact in the field of large‐scale structure determination.
The new double crystal ultra‐small‐angle neutron scattering instrument Kookaburra, currently under construction at the ANSTO OPAL reactor, will allow characterization of microstructures covering length scales in the range of 0.1 to 10 µm. Using the 002 and 004 reflections of a doubly curved mosaic highly oriented pyrolytic graphite premonochromator crystal at a fixed Bragg angle of 45° in conjunction with two pairs of Si(111) and Si(311) quintuple‐reflection channel‐cut crystals will allow operation of the instrument at two different wavelengths, thus optimally accommodating weakly and strongly scattering samples in one sample position. The versatility, the estimated neutron fluxes and the low background noise of Kookaburra suggest that this state‐of‐the‐art instrument will have a major impact in the field of large‐scale structure determination.
A time-of-flight neutron reflectometer is to be built at the new 20 MW research reactor (OPAL) in Sydney. The instrument will be positioned at the end of a curved supermirror neutron guide that will provide optimal transmission of cold neutrons (2-20 Å ) while removing fast neutrons and high-energy g-rays.The reflectometer will utilise a white neutron beam that will be pulsed using a series of boron coated disc choppers. Typically three angle settings will be required to collect a complete reflectivity profile (from Q z ¼ 0.005-0.5 Å 21 ). The new instrument will operate with a vertical scattering plane, making it suitable for both solid and "free-liquid" surfaces. The instrument will also be capable of producing a spinpolarized neutron beam making provision for polarized neutron reflectometry studies. Detection of the reflected neutrons will take place using a 2-dimensional 3 He delay-line detector with high-speed data acquisition electronics.
This review presents the implementation and full characterization of the polarization equipment of the time-of-flight neutron reflectometer PLATYPUS at the Australian Nuclear Science and Technology Organisation (ANSTO). The functionality and efficiency of individual components are evaluated and found to maintain a high neutron beam polarization with a maximum of 99.3% through polarizing Fe/Si supermirrors. Neutron spin-flippers with efficiencies of 99.7% give full control over the incident and scattered neutron spin direction over the whole wavelength spectrum available in the instrument. The first scientific experiments illustrate data correction mechanisms for finite polarizations and reveal an extraordinarily high reproducibility for measuring magnetic thin film samples. The setup is now fully commissioned and available for users through the neutron beam proposal system of the Bragg Institute at ANSTO.
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