The technology of applying a silver coating on fabric is presented. Tissue is wetted with a solution of copper sulphate, which is then reduced to metal-phosphide by phosphine treatment. Wetting can be carried out by immersing the fabric in a copper sulphate solution or spraying the solution onto the fabric using a sprayer. The subsequent processing step is the immersion of the fabric in a solution of silver nitrate, during this copper phosphide is transformed to a silver coating. The developed technology allows achieving a good grip of the fabric with a continuous silver films with a thickness from 40 to 600 nm. Using copper sulphate spray, coatings consisting of individual dots or clusters of silver were obtained. The silver coated tissues exhibited antimicrobial activity even after 10 washing.
Microencapsulation of vitamin E directly from oil-in-water (o/w) emulsions was carried out by means of a novel practically relevant approach. For the first time, a preformed polyelectrolyte-surfactant complex (sodium polystyrene sulfonate/dodecyl trimethyl ammonium bromide) was simultaneously used as an electrosteric emulsion stabilizer and as a charged precursor for the following build up of microcapsules. Subsequently, a layer-by-layer technique was applied to emulsions leading to the formation of core-shell microcapsules with oily cores and polyelectrolyte shells. The effect of the complexes on the process of emulsion formation and on the stability and characteristics of the resulting emulsions was investigated by measurements of dynamic and equilibrium interfacial tension, size distribution (DLS) and interfacial charge (zeta-potential). The resulting microcapsules were characterized by confocal laser scanning microscopy (CLSM), Cryo-SEM, size distribution and zeta-potential measurements on each stage of the shell assembly. The release kinetics of vitamin E was monitored during the consecutive steps of the encapsulation procedure using UV-vis spectroscopy and showed the progressive enhancement of sustainability. The developed approach may be promising for the practical use in the cosmetic and food industry.
Metallization of dielectrics a new physicochemical, mechanical and decorative properties is give to them 1-7. Depending on the type of dielectric material and on the aims to be coated, have been proposed various methods of metallization, among which was the largest use of chemical-electrolytic metallization 3,4. For create a conductive layer in this process the dielectric surface is activated by formation of a catalytic centers, which are then coated by chemical means. At that the active centers consisting of easily reduce metals atoms (copper, silver, palladium), through reduction of metal ions (adsorbed on the surface of dielectric material) by water-soluble or gaseous reducing agent are formed 1-7. As gaseous reducing agent most commonly used hydrogen, and the reduction reaction at high order of several hundred degrees temperature is carried out.
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