Normalizing is an effective heat treatment in improving the microstructure and developing the mechanical properties of micro-alloyed steel. The normalizing parameters such as temperature and holding time are the main keys to microstructure and mechanical properties controlling. Therefore, obtaining an optimum combination of mechanical properties must be subjected to an ideal combination of these parameters. Furthermore, adjusting the optimum normalizing parameters must be considered for every chemical composition depending on the critical transformation temperatures. In this work, four micro-alloyed steel alloys containing V (0.008-0.1wt %) and Ti (0.002-0.072) were held on different normalizing temperatures for 30 minutes. The first holding temperature was carried out just above the Ac3 temperature and the second was carried out above the Ac3 by 100°C (Ac3+100°C). With the controlled normalizing condition, V-Ti-micro-alloyed steel alloy has produced an ultra-fine structure of grain size 2.2 microns and combined high strength of 725 MPa YS, 1058 MPa UTS and good ductility of 20%.
This work aims at designing and developing low carbon steel alloys to meet the high tensile strength, high ductility and high impact toughness properties. The effect of solid solution mechanism, precipitation hardening, as well as grain refinement were developed with different Manganese content (0.78-2.36wt%) combined with Vanadium(0.008-0.1wt%) and Titanium (0.002-0.072wt%) microalloying additions. The controlled thermo-mechanical treatments and chemical compositions play a big role in developing the microstructure and the corresponding mechanical properties. Therefore, the studied chemical compositions were treated thermo-mechanically by two different ways of changing start and finish forging temperatures with subsequent air cooling. The first way by start forging from 1050 to 830oC and the second from 950 to730oC. The second way of forging process developed finer grain sizes and higher ultimate tensile strengths for all the studied steel alloys. In spite of finer grain sizes, the impact toughness value was lower in the second regime due to detrimental influence of precipitation strengthening in the ferrite. A combination of 544 MPa yield strength, 615 MPa ultimate tensile strength, 20% elongation and 138 Joule impact toughness has been attained.
The effects of load and temperature on wear behavior of 6061 Aluminum alloy matrix composite reinforced with 20% Al2O3 (submicron) particulates against AISI 4041 steel disc were studied at elevated temperatures ranging from 25oC to 300oC. Mild and severe wear regions separated by a transition region were observed at all temperatures with a difference of two orders of magnitude between mild and severe wear. The critical loads observed at 100oC, 200oC and 300oC were 40 N (2 MPa), 30 N (1.53 MPa) and 15 N (0.76 MPa) respectively indicating that wear resistance of the composite decreases with increase in temperature. Scanning electron microscopy revealed that wear was accompanied by extensive thermal softening of the matrix, in addition to particulate fracture due to high shear strain generated from the contacts and material transfer to the counterface. The wear rates were reduced in the mild wear regime due to oxidation of the iron counterface and deposition of oxides on the contact surfaces evident by EDS analysis.
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