BACKGROUND: Zirconia is a commonly used ceramic for fixed full-ceramic restorations. Porcelain-fused-to-metal restorations applied for bruxers are often very quickly destroyed by this group of patients.
OBJECTIVE: The aim of this study was to investigate the influence of accelerated aging tests on BruxZir HT 2.0 zirconia.
METHODS: Zirconia samples were prepared with ISO 13356:2013 and ISO 14704:2008 protocol recommendations. The ageing conditions were times of 2.5, 5 and 10 hours, and pressure of 0.2 MPa and a temperature of 134°C.
RESULTS: The correlation between ageing time and mechanical properties, particularly hardness, was difficult to find, while correlations between hardness and the surface topography and fracturing were clear.
CONCLUSION: On the basis of the conducted research, it can be stated that BruxZir HT 2.0 zirconia meets the technical requirements for medical grade zirconia used in dental technology. Future investigations should include phase composition research.
Purpose: This part of the study focuses on the influence of zirconia heat treatment for surface morphology, phase composition and mechanical properties
Methods: Zirconia samples was prepared with ISO 13356:2013 and ISO 14704:2008 recommendations. X-ray diffraction, observations (SEM) and (AFM), microhardness (Olivera & Phara method), and static bending test (4PBT) were taken.
Results: characterization of YSZ and high temperature heat treatment has clearly shown that the aging process influences the change in phase composition of the material, significantly worsening the topography. In turn, re-treatment of the high temperature made after the artificial aging process results in reverse transformation of the desired tetragonal phase, but does not affect the improvement of surface morphology.
Conclusions: The research made it possible to assess the negative impact of the zirconium oxide aging simulation process. Because of the failure to achieve the intended results, it was also proved that the high-temperature re-processing was not appropriate.
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