Purpose The purpose of this paper is to assess the possibility of cross-linking silk fabric using citric acid (CA) as the cross-linking agent and nano-TiO2 (NTO) particles as a catalyst at low temperature and under UV irradiation. This paper also assesses the possibility of treated samples with suitable combinations of CA and NTO to impart multiple functional properties such as self-cleaning and antimicrobial properties. Design/methodology/approach In this research, ß-cyclodextrin (ß-CD) grafted onto silk fabric using CA as a crosslinking agent and NTO particles as a catalyst through a pad-dry-cure technique and with UVA irradiation. The effects of different concentrations of CA, ß-CD and NTO particles on some properties of the treated samples are evaluated, and the optimum finishing conditions are obtained. The author also investigated the washing durability of the modified product after ten times of washing. Findings The results showed that CA plays the role of a linking agent through an esterification reaction with the hydroxyl groups of both ß-CD and silk fabrics and improves the durability of materials on the textile surface. Also, the silk fabrics treated with CA only were found to have excellent photocatalytic properties and better antibacterial activity than the control sample and the fabrics treated with a mixture of ß-CD/CA. Originality/value This study was conducted to achieve multiple functions such as antibacterial and photocatalytic activities, good dry crease recovery angle and wet crease recovery angle behavior without a significant adverse effect on the Yellowness index and tensile properties for treated silk fabrics.
Purpose The purpose of this study is the chemical grafting of β-Cyclodextrin (β-CD) onto silk fabrics by the use of butane tetracarboxylic acid (BTCA) as a crosslinking agent and nano-TiO2 (NTO) as a catalyst. The effects of different parameters involved in this particular process, e.g. β-CD, BTCA and NTO concentrations, are examined using the artificial neural network (ANN). The method is evaluated for its ability to predict certain properties of treated fabrics, including grafting yield, dry crease recovery angle (DCRA) and wet crease recovery angle (WCRA), tensile strength, elongation at break and methylene blue dye absorption. Design/methodology/approach This study was conducted to describe the cross-linking of silk with 1,2,3,4-BTCA as a crosslinking agent in a wet state at low temperatures using NTO catalyst to improve the dry and wet wrinkle recovery (DCRA and WCRA) of silk fabrics. An ANN was also used to model and analyze the effects of BTCA, β-CD and NTO concentrations on the grafting percentage and some properties of the treated samples. Findings According to the results, the wet and dry wrinkle recovery of the silk fabrics was improved for about 38% and 11%, respectively, as compared to the non-cross-linked fabrics, without significantly affecting the tensile strength retention of the fabrics. Originality/value This research model and analyze the effects of BTCA, β-CD and NTO concentrations on the grafting percentage and some properties of the treated samples for the first time.
Purpose This paper aims to extracted sericin from the cocoons of Bombyx mori silkworms, and sericin powder was applied onto drawn textured polyethylene terephthalate (PET) yarns as a spin finish. The reactivity on the surface of PET yarns was analyzed through Fourier transform infrared spectrophotometry–attenuated total reflectance (FTIR-ATR) and dyeing with methylene blue as a reactive dye. Also, investigations were conducted on the effects of sericin, citrc acid (CA) (as a crosslinking agent), and sodium hypophosphite (as a catalyst) concentrations on some properties of false-twist textured PET yarns. Design/methodology/approach A false-twist texturing machine (Scragg-Shirley minibulk, England) was used with the draw ratio of 1.05, heating temperature of 120°C, texturing speed of 100 m min−1 and applied twist of 3,000 TPM. The aqueous extraction of sericin was carried out by the boiling of the raw silk in distilled water with L:R: 40:1 for 120 min. The aqueous solution was filtered with a filter paper to remove the impurities and insoluble fibroin. Finally, the sericin solution was freeze-dried to obtain the sericin powder. The sericin solution was applied on the drawn textured PET yarns using the “pad-dry-cure” method. Findings Sericin fixation onto the PET yarns was confirmed by FTIR-ATR. The results showed that there were no significant changes in the tensile strength, linear density, crimp contraction and crimp modulus, elongation at break and shrinkage. In contrast, a substantial increase was observed in moisture regain, vertical wicking, dye uptake and ultraviolet protection. There was also a reduction just in the electrical resistivity, in the presence of sericin. Originality/value Although sericin has been known to have numerous beneficial properties, its application in textile industry as a spin finish has not been reported yet.
Purpose This study aims to enhance the dyeability of polyester fabrics with turmeric natural dyes through plasma and alkaline treatments. The aim is to achieve better color strength in dyed samples without significant changes in their other properties. This is done while the weight loss is kept in a range with no considerable effect on those properties. Design/methodology/approach The surface of a poly(ethylene terephthalate) fabric was modified using oxygen plasma at a low temperature. The alkaline hydrolysis of that polyester fabric was also done through treating it with an aqueous sodium hydroxide (NaOH) solution. The untreated and treated polyester fabrics were studied for the changes of their physical characteristics such as weight loss, wetting behavior, strength loss, bending length, flexural rigidity and K/S and wash fastness. The samples were treated with plasma and sodium hydroxide and dyed with a turmeric natural dye. Findings In comparison to the untreated sample, the plasma-treated, alkaline-treated and plasma treatment followed by alkaline hydrolysis polyester experienced 9.3%, 68.6% and 102.3% increase in its color depth as it was dyed with a turmeric natural dye, respectively. The plasma treatment was followed by alkaline hydrolysis. The improvement in the color depth could be attributed to the surface modification. Originality/value In this paper, investigations were conducted of the separate effects of plasma treatment and alkaline hydrolysis as well as their synergistic effect on the dyeing of the polyester fabric with a natural dye obtained from turmeric.
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