Reaction of Ni(ClO4)2•6H2O with a tripodal ligand having two di(tert-butyl)phenol moieties, H2tbuL, and 1 equivalent of triethylamine in CH2Cl2/CH3OH (1:1 v/v) under N2 gave a Ni(II)-(phenol)(phenolate) complex, [Ni(HtbuL)(CH3OH)2]ClO4. Formation of...
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