Amorphous and liquid Fe80B20 and Fe75B25 alloys are investigated by means of X‐ray diffraction. The interference functions of the amorphous and liquid state are similar but the quantitative differences cannot be explained by a temperature factor only. Interference functions are calculated for microcrystalline Fe3B‐clusters in dependence on size. The theoretical curves are similar for a diameter of 0.6 nm to that of liquid FeB and for a diameter of 0.8 nm to that of amorphous FeB.
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