The volumetric liquid-phase mass transfer coefficient, k L a, was determined by absorption of oxygen in air using six different carboxy-methyl cellulose (CMC) solutions with different rheological values in three phase spout-fluid beds operated continuously with respect to both gas and liquid. Three cylindrical columns of 7.4 cm, 11.4 cm, and 14.4 cm diameters were used. Gas velocity was varied between 0.00154±0.00563 m/s, liquid velocity between 0.0116±0.0387 m/s, surface tension between 0.00416±0.0189 N/m, static bed height between 6.0±10.8 cm, and spherical glass particles of 1.75 mm diameter were used as packing material. A single nozzle sparger of 1.0 cm diameter was used in the spouting line. The volumetric mass transfer coefficient was found to increase with gas velocity, liquid velocity, and static bed height and to decrease with the increase of the effective liquid viscosity of the CMC solution. A dimensionless correlation was developed and compared with those listed in the literature.
Following on from the work of Anabtawi et al. (2003), this study examined how the volumetric liquid-phase mass transfer coefficient, k L a, of oxygen in air in threephase spout-fluid beds was affected by varying the system parameters of bed height, bed diameter, gas velocity, and liquid velocity. The liquid used was 0.1% CMC solution, displaying a pseudo-plastic rheology, with 1.75 mm glass spheres as packing. The values of the Sherwood number were lower than in previous studies (Anabtawi et al., 2003), in the range 9,000-186,000. Gas velocity had a similar effect on k L a as in a bubble column, with results also giving good agreement with previous work on two-phase and three-phase spouted bed systems. The correlation obtained for the effect of liquid velocity on k L a compared well with that of Schumpe et al. (1989). An increase in the height of packing increased k L a to the power of 0.319, with an increase in column diameter also causing an increase in k L a, which is in agreement with the results of Akita and Yoshida (1973).
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