α1-Adrenoceptor Agonists: The Identification of Novel α1A Subtype Selective 2′-Heteroaryl-2-(phenoxymethyl)imidazolines

Bis[2-(4,5-dihydro-1H-imidazol-2-yl)phenolato-κ2N,O]nickel(II)

“…2-(4,5-Dihydro-1H-imidazol-2-yl)phenol (58 mg, 0.37 mmol), which was prepared according to the literature method (Bishop et al, 2002), and nickel(II) perchlorate hexahydrate (65 mg, 0.18 mmol) were dissolved separately in methanol (5 ml). The solutions were mixed and stirred for 0.5 h. The clear solution was then kept at room temperature.…”

Bis[μ-2-(1H-imidazol-2-yl)phenolato]bis[chloromethanolcopper(II)]

“…Equimolar quantities of 2-(1H-imidazol-2-yl)phenol, prepared according to the literature method of Bishop et al (2002), and anhydrous copper chloride were dissolved separately in methanol (10 ml). The solutions were mixed and stirred for 1 h. Dark-brown crystals were obtained after 3 d by slow evaporation of the solution at room temperature.…”

Tris[2-(1H-imidazol-2-yl)phenolato-κ2N,O]chromium(III) methanol trisolvate

“…Each nest is formed by six molecules bridged by 12 methanol molecules. Experimental 2-(1H-Imidazol-2-yl)phenol (58,7 mg, 0.37 mmol), which was prepared according to the literature method (Bishop et al, 2002), and chromium(III) nitrate hydrate (48 mg, 0.12 mmol) were dissolved separately in methanol (5 ml). The solutions were mixed and stirred for 1 h. The clear solution was kept at room temperature and the solvent was evaporated slowly.…”