XRD, FE-SEM, FT-IR and ESR studies of cation deficient potassium tris(oxalato)ferrate(III)trihydrate

Growing a Display Crystal of Recycled Potassium Tris(oxalato)ferrate(III) Trihydrate

“…The preparation of potassium tris­(oxalato)­ferrate­(III) trihydrate is a well-known coordination chemistry experiment used in general or upper-level chemistry laboratories. − This material can be synthesized , from Fe­(NH 4 ) 2 (SO 4 ) 2 ·6H 2 O via an iron­(II) oxalate intermediate, analyzed for its oxalate or iron content in subsequent experiments, or studied for its photochemical, , equilibrium, and X-ray diffraction properties.…”