“…6, the pressure in zones A and B was gradually ramped up from 0 to 18 k psi synchronously. The pressure in zone B was then increased while maintaining pressure in zone A; the separation force F Sep [see (6)] was subsequently slowly increased in a controlled manner to understand the threshold value when the piston began to move. During the process of increasing pressure in zone B, the valve of zone A was turned off, becoming a closed volume.…”