When transition-metal catalysis meets electrosynthesis: a recent update

Lian, Fei; Li, Jiu-Ling; Xu, Kun

doi:10.1039/d4ob00484a

Org. Biomol. Chem.

2024

DOI: 10.1039/d4ob00484a

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When transition-metal catalysis meets electrosynthesis: a recent update

Fei Lian,

Jiu-Ling Li,

Kun Xu

Abstract: While aiming at sustainable synthesis, organic electrosynthesis has attracted increasing attention in the past few years. In parallel, with a deeper understanding of catalyst and ligand design, 3d transition-metal catalysis...

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Mn-Catalyzed Electrooxidative Radical Cascade Cyclization for the Synthesis of 6-Phosphorylated Quinoxalino[2,1-b]quinazolin-12-ones

Xie,

Duan,

Cao

et al. 2024

J. Org. Chem.

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Due to their important potential medicinal value, chemists are pursuing mild and efficient methods to synthesize structurally diverse quinazolinone derivatives. In this paper, a series of isocyano-tethered N-aryl quinazolinones were designed and synthesized to conduct electrocatalytic radical cascade cyclization reactions with phosphine oxides by utilizing inexpensive MnII salt as the catalyst. The desired 6-phosphorylated quinoxalino[2,1-b]quinazolin-12-ones were obtained in moderate to good yields.

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Mn-Catalyzed Electrooxidative Radical Cascade Cyclization for the Synthesis of 6-Phosphorylated Quinoxalino[2,1-b]quinazolin-12-ones

Xie,

Duan,

Cao

et al. 2024

J. Org. Chem.

View full text Add to dashboard Cite

show abstract

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When transition-metal catalysis meets electrosynthesis: a recent update

Abstract: While aiming at sustainable synthesis, organic electrosynthesis has attracted increasing attention in the past few years. In parallel, with a deeper understanding of catalyst and ligand design, 3d transition-metal catalysis...

Cited by 1 publication

References 97 publications

Mn-Catalyzed Electrooxidative Radical Cascade Cyclization for the Synthesis of 6-Phosphorylated Quinoxalino[2,1-b]quinazolin-12-ones

Mn-Catalyzed Electrooxidative Radical Cascade Cyclization for the Synthesis of 6-Phosphorylated Quinoxalino[2,1-b]quinazolin-12-ones

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