“…Each factor was run at three levels so that the experiment was a 3 3 factorial design with two replicates as per the Box Behnken design of experiment. 14 The samples were prepared after randomisation according to a random number table and the sequence of sample production comprised the process variables given at serial numbers 2,4,9,11,6,5,15,14,1,12,7,8,3,10,13. The reasons for randomisation were an effective statistical analysis and the validity of the inference drawn.…”