2023
DOI: 10.1002/chem.202301934
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Visible Light and Triselenium Dicyanide (TSD): New Horizons in the Synthesis of Organic Selenocyanates

Abstract: Herein we describe a new method for the synthesis of α‐carbonyl selenocyanates by reacting triselenium dicyanide (TSD) and styrenes under blue light irradiation and O2 atmosphere. The reactions are triggered by the formation of Se‐centered radical species, followed by the addition/oxidation of the styrene π‐bond. α‐Carbonyl selenocyanates and α‐hydroxy selenocyanates were obtained in moderate to excellent yields from aryl‐ and alkyl‐substituted alkenes, respectively. It was demonstrated that α‐carbonyl selenoc… Show more

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