“…To achieve the experimental goal while saving energy, the process parameters of the calcination stage were set as follows: the grapefruit peel loaded with precursor was calcined in a muffle furnace under an air atmosphere, with the temperature rising at a rate of 5 °C min −1 from room temperature to 550 °C, followed by a three-hour heat preservation phase, and then naturally cooled to room temperature. According to the added amount of TBOT, the resultant samples were recorded as CPK-TiO 2 -x (x = 10, 15,20,25). In order to facilitate comparison, control samples without grapefruit peel templates were also prepared under the same conditions, referred to as N-TiO 2 -x (x = 10, 15, 20, 25).…”