Validation of QuEChERS-based UPLC-MS/MS method for determination of quinoid niclosamide (LDS) residue in water, soil and rice samples

Kaium, Abdul; Cao, Junli; Liu, Xingang; Dong, Fengxia; Xu, Jun; Wu, Xiaohu; Zheng, Yongquan

doi:10.1080/03067319.2018.1487062

Cited by 8 publications

(3 citation statements)

References 16 publications

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“…Therefore, its recovery study from animal tissue is essential. The maximum residue level as per Australian standards is 0.01 mg/kg [ 32 ]. Bayluscide contains niclosamide ethanolamine, a registered molluscicide for controlling sea lamprey populations [ 33 ].…”

Section: Analytical Methods For Estimation Of Niclosamidementioning

confidence: 99%

“…This may lead to the entry of mobile chemicals, including pesticides such as niclosamide which pose a risk to humans where underground water is used for drinking [ 36 ]. Hence, environmental monitoring of these trace contaminants is crucial, and there are a couple of sophisticated techniques to analyze niclosamide and its degradation products in water, wastewater, and sludge [ 32 , 36 ].…”

Section: Analytical Methods For Estimation Of Niclosamidementioning

confidence: 99%

“…The analytical chromatographic methods covered in this section for analyzing niclosamide are HPLC, UPLC, LC-PDA, LC-UV, preparative-HPLC, and LC-light scattering detector. There are 11 HPLC-based methods [30,32,36,37,[39][40][41][42][43][44][45] with various detectors for analyzing niclosamide, summarized in Table 1.…”

Section: Analytical Chromatographymentioning

confidence: 99%

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Techniques for analytical estimation of COVID‐19 clinical candidate, niclosamide in pharmaceutical and biomedical samples

Gupta

Bharate

2022

Separation Science Plus

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Niclosamide is a well‐known broad‐spectrum antiparasitic drug used for human as well as veterinary tapeworm infections. Recently, it attracted attention as an antiviral agent for treating coronavirus disease 2019. It is administered orally in humans to treat tapeworm infections. Furthermore, it is a registered pesticide and molluscicide to control infections in the aquaculture industry. Its chronic environmental exposure has potential toxicities when such contaminated seafood is consumed. Therefore, monitoring its residual concentration in food products (seafood, water, water waste, etc.) and pharmaceuticals (active pharmaceutical ingredients, bulk drugs, and formulations) is imperative. The present review critically investigates the sophisticated techniques employed for analyzing niclosamide, its degradation products, and metabolites in various samples and matrices. The future scope for green analytical methods, green sample extraction and preparation is also deliberated.

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Section: Analytical Methods For Estimation Of Niclosamidementioning

confidence: 99%