Using infrared spectroscopy in combination with multivariate data analysis to predict residual strength of carbon fiber reinforced polymers after one‐sided thermal loading

Abstract

In this study, structural, mechanical, and chemical changes of one-sided thermally loaded carbon fiber reinforced polymers (CFRPs) are investigated. The aim is to test and reliably predict residual strength and delamination depth by using infrared spectroscopy. CFRP of different thicknesses (HexPly ® 8552/ IM7) were irradiated at varying heat fluxes over various time intervals. The inhomogeneously distributed matrix degradation was analyzed by means of attenuated total reflection Fourier transform infrared spectroscopy with a depth resolution of 0.2 mm. Residual interlaminar shear strength (ILSS) was determined and microfocused computed X-ray tomography was used to measure the delamination depth. Principal component analyses were performed to show which information in the infrared spectra is affected by thermal loading. Furthermore, the combination of spectra taken at different depths of the CFRP can be used to develop partial least squares regression models to predict ILSS and delamination depth. Despite an inhomogenous distribution of thermal damage, precise predictions of ILSS and delamination depth with models considering varying sample thicknesses and heat fluxes were achieved.

Temporal residual spontaneous cure in L‐shaped composites structures: The influence of angular stacking sequence, autoclave cooling rate cycle, and thickness

“…They concluded that laminates with graphene structures had better mechanical properties than laminates without them. Vetter et al [ 10 ] studied the structural, mechanical, and chemical changes of one‐sided thermally loaded carbon fiber reinforced polymers. These additional reinforcement structures seem to have influence on the residual curing mechanics of these polymeric matrices.…”