Use of circular dichroism measurements to determine the formation constant of the complex between an optically active benzo-15-crown-5 and sodium ion

Mack, Mark P.; Hendrixson, Richard R.; Palmer, Richard A.; Ghirardelli, Robert G.

doi:10.1021/ja00440a068

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Cited by 41 publications

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“…(2S,2'S)-l,l'-(+)-Oxybis (2-propanol) was prepared by the outline given by Ghirardelli and Palmer. 14 By use of the procedure above, 56.2 g (0.351 mol) of (S)-2-[(tetrahydro-2-pyranyl)oxy]-l-propanol in 150 mL of dry THF was added to a solution of 9.6 g (0.4 mol) of sodium hydride in 300 mL of dry THF. After 0.5 h, 110. was worked up in the usual manner to yield 119 g of the crude THP ether.…”

Section: Methodsmentioning

confidence: 99%