Abstract:Metal three-dimensional (3D) printing includes a vast number of operation and material parameters with complex dependencies, which significantly complicates process optimization, materials development, and real-time monitoring and control. We leverage ultrahigh-speed synchrotron X-ray imaging and high-fidelity multiphysics modeling to identify simple yet universal scaling laws for keyhole stability and porosity in metal 3D printing. The laws apply broadly and remain accurate for different materials, processing… Show more
“…Lastly, the velocity (V) was the only parameter that had a moderate impact on the keyhole width, with all other parameters having poor correlation. Furthermore, the addition of feature P∕ √ VD highlights strong positive dependency with depth, which agrees with the work conducted by Gan et al [25] where they found that keyhole depth scales linearly with P∕ √ VD. It should be noted that the size of the dataset only consists of 14 X-ray imaging experiments, so the trends we observed are indicative rather than definitive.…”
Section: Spearman's Correlationsupporting
confidence: 91%
“…When compared to previous work by Gan et al [25], the current study shows that depth is more strongly correlated with P/VD than with P∕ √ VD . One thing to note is that they used the absorbed power in the material which they were able to estimate using absorptivity simulations, rather than the raw laser power, which is what is used in this work.…”
During laser melting of metals, localized metal evaporation resulting in the formation of a keyhole shaped cavity can occur if processing conditions are chosen with high power density. An unstable keyhole can have deleterious effects in certain applications (e.g., laser powder bed fusion) as it increases the likelihood of producing defects such as porosity. In this work, we propose a pipeline that enables complete segmentation and extraction of various geometric features in keyholing conditions. In situ synchrotron high-speed X-ray visualization at the Advanced Photon Source provides large datasets of experimental images with a high spatio-temporal resolution across a range of laser parameters for Ti-6Al-4V. Computer vision image processing techniques were used to extract time-resolved quantitative geometric features (e.g., depth, width, front wall angle) throughout keyhole evolution which were subsequently analyzed to understand the relationship between the variation of local keyhole geometry and processing conditions. This analysis is the first to employ a data-driven approach to further our understanding of the keyholing process regime.
“…Lastly, the velocity (V) was the only parameter that had a moderate impact on the keyhole width, with all other parameters having poor correlation. Furthermore, the addition of feature P∕ √ VD highlights strong positive dependency with depth, which agrees with the work conducted by Gan et al [25] where they found that keyhole depth scales linearly with P∕ √ VD. It should be noted that the size of the dataset only consists of 14 X-ray imaging experiments, so the trends we observed are indicative rather than definitive.…”
Section: Spearman's Correlationsupporting
confidence: 91%
“…When compared to previous work by Gan et al [25], the current study shows that depth is more strongly correlated with P/VD than with P∕ √ VD . One thing to note is that they used the absorbed power in the material which they were able to estimate using absorptivity simulations, rather than the raw laser power, which is what is used in this work.…”
During laser melting of metals, localized metal evaporation resulting in the formation of a keyhole shaped cavity can occur if processing conditions are chosen with high power density. An unstable keyhole can have deleterious effects in certain applications (e.g., laser powder bed fusion) as it increases the likelihood of producing defects such as porosity. In this work, we propose a pipeline that enables complete segmentation and extraction of various geometric features in keyholing conditions. In situ synchrotron high-speed X-ray visualization at the Advanced Photon Source provides large datasets of experimental images with a high spatio-temporal resolution across a range of laser parameters for Ti-6Al-4V. Computer vision image processing techniques were used to extract time-resolved quantitative geometric features (e.g., depth, width, front wall angle) throughout keyhole evolution which were subsequently analyzed to understand the relationship between the variation of local keyhole geometry and processing conditions. This analysis is the first to employ a data-driven approach to further our understanding of the keyholing process regime.
“…Cunningham et al 25 reported a nonlinear relationship between the FKW angle and the power density ( ), which changes with the laser scan velocity as well as powder materials. Gan et al 44 found that the tangent of FKW angle is approximately proportional to the “keyhole number ” ( ), which is a scaled version of the normalised enthalpy. Here, we find even stronger agreement between the FKW angle and the normalised enthalpy product (Supplementary Fig.…”
Section: Resultsmentioning
confidence: 99%
“…Within the keyhole-melting regime, recent studies have reported a sharp transition between stable and unstable keyhole melting, typically defined by the onset of keyhole porosity 16 , 25 , 44 . From our data, we observed that the threshold for this transition can vary significantly between alloys.…”
Keyhole porosity is a key concern in laser powder-bed fusion (LPBF), potentially impacting component fatigue life. However, some keyhole porosity formation mechanisms, e.g., keyhole fluctuation, collapse and bubble growth and shrinkage, remain unclear. Using synchrotron X-ray imaging we reveal keyhole and bubble behaviour, quantifying their formation dynamics. The findings support the hypotheses that: (i) keyhole porosity can initiate not only in unstable, but also in the transition keyhole regimes created by high laser power-velocity conditions, causing fast radial keyhole fluctuations (2.5–10 kHz); (ii) transition regime collapse tends to occur part way up the rear-wall; and (iii) immediately after keyhole collapse, bubbles undergo rapid growth due to pressure equilibration, then shrink due to metal-vapour condensation. Concurrent with condensation, hydrogen diffusion into the bubble slows the shrinkage and stabilises the bubble size. The keyhole fluctuation and bubble evolution mechanisms revealed here may guide the development of control systems for minimising porosity.
“…Once the peak temperature is higher than the boiling point of the material, due to the multireflection of the laser beam between the walls of the depression, the keyhole depression deepens, resulting in rising absorbed power [84,85]. In this situation, the absorptivity (called absorptivity 1 in our benchmark), η, can be expressed as [86]:…”
Section: Atomic Volume Electron Affinitymentioning
Characterizing meltpool shape and geometry is essential in metal Additive Manufacturing (MAM) to control the printing process and avoid defects. Predicting meltpool flaws based on process parameters and powder material is difficult due to the complex nature of MAM process. Machine learning (ML) techniques can be useful in connecting process parameters to the type of flaws in the meltpool. In this work, we introduced a comprehensive framework for benchmarking ML for melt pool characterization. An extensive experimental dataset has been collected from more than 80 MAM articles containing MAM processing conditions, materials, meltpool dimensions, meltpool modes and flaw types. We introduced physics-aware MAM featurization, versatile ML models, and evaluation metrics to create a comprehensive learning framework for meltpool defect and geometry prediction. This benchmark can serve as a basis for melt pool control and process optimization. In addition, data-driven explicit models have been identified to estimate meltpool geometry from process parameters and material properties which outperform Rosenthal estimation for meltpool geometry while maintaining interpretability.
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