Ultrasound-mediated synthesis of N,N-bis(phenacyl)aniline under solvent-free conditions

Jianguo, He; Shi, Lei; Liu, Sijie; Jia, Peng; Wang, Juan; Hu, Ruisheng

doi:10.1007/s00706-013-0978-7

Cited by 5 publications

(1 citation statement)

References 24 publications

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“…The title compound was synthesized using the reported procedure (He et al, 2014), and pale-yellow needle-like crystals were obtained upon slow evaporation from an ethanol/ water (4:1) homogeneous solution at room temperature.…”

Section: Synthesis and Crystallizationmentioning

confidence: 99%

Crystal structure and Hirshfeld surface analysis of 2,2′-(phenylazanediyl)bis(1-phenylethan-1-one)

et al. 2022

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The whole molecule of the title compound, C22H19NO2, is generated by twofold rotational symmetry. The N atom exhibits a trigonal-planar geometry and is located on the twofold rotation axis. In the crystal, molecules are linked by C—H...O contacts with R 2 2(12) ring motifs, and C—H...π interactions, resulting in ribbons along the c-axis direction. van der Waals interactions between these ribbons consolidate the molecular packing. Hirshfeld surface analysis indicates that the greatest contributions to the crystal packing are from H...H (45.5%), C...H/H...C (38.2%) and O...H/H...O (16.0%) interactions.

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Section: Synthesis and Crystallizationmentioning

confidence: 99%

Crystal structure and Hirshfeld surface analysis of 2,2′-(phenylazanediyl)bis(1-phenylethan-1-one)

et al. 2022

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Advances in Green Organic Sonochemistry

Draye

Kardos

2016

Top Curr Chem (Z)

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Over the past 15 years, sustainable chemistry has emerged as a new paradigm in the development of chemistry. In the field of organic synthesis, green chemistry rhymes with relevant choice of starting materials, atom economy, methodologies that minimize the number of chemical steps, appropriate use of benign solvents and reagents, efficient strategies for product isolation and purification and energy minimization. In that context, unconventional methods, and especially ultrasound, can be a fine addition towards achieving these green requirements. Undoubtedly, sonochemistry is considered as being one of the most promising green chemical methods (Cravotto et al. Catal Commun 63: 2-9, 2015). This review is devoted to the most striking results obtained in green organic sonochemistry between 2006 and 2016. Furthermore, among catalytic transformations, oxidation reactions are the most polluting reactions in the chemical industry; thus, we have focused a part of our review on the very promising catalytic activity of ultrasound for oxidative purposes.

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LC–MS/MS analysis of the central energy and carbon metabolites in biological samples following derivatization by dimethylaminophenacyl bromide

Willacey

Naaktgeboren

Moreno

et al. 2019

Journal of Chromatography A

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Ultrasound-mediated synthesis of N,N-bis(phenacyl)aniline under solvent-free conditions

Cited by 5 publications

References 24 publications

Crystal structure and Hirshfeld surface analysis of 2,2′-(phenylazanediyl)bis(1-phenylethan-1-one)

Crystal structure and Hirshfeld surface analysis of 2,2′-(phenylazanediyl)bis(1-phenylethan-1-one)

Advances in Green Organic Sonochemistry

LC–MS/MS analysis of the central energy and carbon metabolites in biological samples following derivatization by dimethylaminophenacyl bromide

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