Two-step combustion synthesis of nanocrystalline Zn1-xMnxFe2O4 (0&lt;x&lt;1) spinel ferrites with linear tuning of magnetic parameters

Martinson, K.D.; Попков, В.И.

doi:10.17586/2220-8054-2021-12-5-634-640

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2022

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Cited by 2 publications

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“…A solution combustion method is advantageous for production of nanocrystalline ferrites with various compositions, including Bi 2 Fe 4 O 9 , at rather high temperature, since a fast combustion reaction process does not contribute to recrystallization particle growth [11][12][13][14][15][16][17][18][19][20][21][22].…”

Section: Introductionmentioning

confidence: 99%

Magnetic properties of nanocrystalline material based on Bi-=SUB=-2-=/SUB=-Fe-=SUB=-4-=/SUB=-O-=SUB=-9-=/SUB=-

Buryanenko

Ломанова

Осипов

et al. 2022

Physics of the Solid State

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Section: Introductionmentioning

confidence: 99%

Magnetic properties of nanocrystalline material based on Bi-=SUB=-2-=/SUB=-Fe-=SUB=-4-=/SUB=-O-=SUB=-9-=/SUB=-

Buryanenko

Ломанова

Осипов

et al. 2022

Physics of the Solid State

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Microwave-Enhanced Crystalline Properties of Zinc Ferrite Nanoparticles

et al. 2022

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Two series of ZnFe2O4 mixed cubic spinel nanoparticles were prepared by a coprecipitation method, where a solution of Fe3+ and Zn2+ was alkalised by a solution of NaOH. While the first series was prepared by a careful mixing of the two solutions, the microwave radiation was used to enhance the reaction in the other series of samples. The effect of the microwave heating on the properties of the prepared particles is investigated. X-ray powder diffraction (XRD), 57Fe Mössbauer spectroscopy and magnetometry were employed to prove the cubic structure and superparamagnetic behavior of the samples. The particle size in the range of nanometers was investigated by a transmission electron microscopy (TEM), and the N2 adsorption measurements were used to determine the BET area of the samples. The stoichiometry and the chemical purity were proven by energy dispersive spectroscopy (EDS). Additionally, the inversion factor was determined using the low temperature Mössbauer spectra in the external magnetic field. The microwave heating had a significant effect on the mean coherent length. On the other hand, it had a lesser influence on the size and BET surface area of the prepared nanoparticles.

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Two-step combustion synthesis of nanocrystalline Zn1-xMnxFe2O4 (0<x<1) spinel ferrites with linear tuning of magnetic parameters

Cited by 2 publications

References 25 publications

Magnetic properties of nanocrystalline material based on Bi-=SUB=-2-=/SUB=-Fe-=SUB=-4-=/SUB=-O-=SUB=-9-=/SUB=-

Magnetic properties of nanocrystalline material based on Bi-=SUB=-2-=/SUB=-Fe-=SUB=-4-=/SUB=-O-=SUB=-9-=/SUB=-

Microwave-Enhanced Crystalline Properties of Zinc Ferrite Nanoparticles

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