“…For the solid-state ligand-exchange step, EDT (98%, Sigma-Aldrich), ammonium chloride (NH 4 Cl, 99.5%, Sigma-Aldrich), ammonium bromide (NH 4 Br, 99%, Sigma-Aldrich), ammonium iodide (NH 4 I, 99%, Sigma-Aldrich), sodium sulfide (Na 2 S, Sigma-Aldrich), acetonitrile (electronic grade, 99.999%, Sigma-Aldrich), and methanol (anhydrous, 99.8%) were used without further purification. The 6-LiXers were synthesized according to a previously reported method ( 52 , 53 ). For FETs, Si wafers ( n ++ , <0.005 ohm) with a thermally grown SiO 2 layer (300 nm) (Namkang Hi-Tech) were used as the substrate.…”