Abstract:Near ambient pressure X-ray photoelectron spectroscopy (nAP-XPS) affords unparalleled insight into the physicochemical processes that drive electrocatalytic devices.1 Studies featuring nAP-XPS span a broad range of materials and reactions, with many focused on thin films or other well-defined materials. Experiments featuring a water vapor atmosphere, or a humidified atmosphere (often with O2 or H2 as the other vapor component) have been effectively used to study the fundamentals of the electrocatalytic reactio… Show more
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