Trace Element Determination by ICP‐AES and ICP‐MS: Developments and Applications Reported During 2006 and 2007

Linge, Kathryn L.

doi:10.1111/j.1751-908x.2008.00917.x

Cited by 17 publications

(8 citation statements)

References 70 publications

(57 reference statements)

Supporting

Mentioning

Contrasting

Order By: Relevance

“…This is the fourth biennial review published in GGR of atomic absorption spectroscopy (AAS), instrumental neutron activation analysis (INAA), and X‐ray fluorescence (XRF) spectrometry (Bédard 2008). However, for the first time, inductively coupled plasma‐atomic emission spectrometry (ICP‐AES), previously covered in a separate review (Linge 2008), has also been included. In order to evaluate the activity of these analytical methods, a search was performed using the online bibliographic database ‘Web of Science’ using ‘atomic absorption’ and the abbreviations ‘INAA’, ‘XRF’ and ‘ICP‐AES’ or ‘ICP‐OES’, limited to analytical chemistry (Table 1).…”

Section: The Number Of Papers and Citations Reported By Web Of Sciementioning

confidence: 99%

GGR Biennial Review: Atomic Absorption, Inductively Coupled Plasma‐Atomic Emission Spectrometry, Neutron Activation Analysis and X‐Ray Fluorescence Spectrometry Review for 2008–2009

Bèdard¹,

Linge²

2010

Geostandard Geoanalytic Res

Self Cite

View full text Add to dashboard Cite

This review describes developments major and in trace element determination using atomic absorption spectroscopy (AAS), inductively coupled plasma‐atomic emission spectrometry (ICP‐AES), instrumental neutron activation analysis (INAA), and X‐ray fluorescence (XRF) spectrometry that were reported in 2008 and 2009. Publication levels were comparable to those of previous years, except for XRF which showed an increase in the number of articles published in the past 2 years. In terms of number of publications and impact, the most active field was AAS, while INAA was the least active. As expected for well‐established and mature methods, novel developments for all four analytical techniques were relatively sparse. For AAS, the most notable publications concerned developments in sample introduction, particularly focussing on solid samples, increasing analyte sensitivity, and higher sample throughput. For ICP‐AES, publication of developments in sample introduction, remediation of matrix effects and calibration continues. Compared with past years, there was a clear focus on sample preconcentration methods, but very few publications reporting new hyphenated speciation methods. For INAA, there were several publications exploring the accuracy and robustness of the method, as well as the requirements for INAA to meet criteria for a primary method of measurement. Two other related techniques, delayed neutron activation analysis, and prompt gamma activation analysis, were also described. Hyphenated XRF techniques showed interesting developments in enabling XRF and XRD analysis on the same spot, and further work characterising and calibrating three‐dimensional micro‐XRF shows promising results for investigating sample heterogeneity.

show abstract

Section: The Number Of Papers and Citations Reported By Web Of Sciementioning

confidence: 99%

GGR Biennial Review: Atomic Absorption, Inductively Coupled Plasma‐Atomic Emission Spectrometry, Neutron Activation Analysis and X‐Ray Fluorescence Spectrometry Review for 2008–2009

Bèdard¹,

Linge²

2010

Geostandard Geoanalytic Res

Self Cite

View full text Add to dashboard Cite

show abstract

“…Despite the availability of advanced analytical instruments, such as atomic absorption spectroscopy (AAS) and inductively coupled plasma‐mass spectrometry (ICP‐MS), sample pretreatment is necessary for preconcentration and purification purposes during heavy metal analysis . It was previously reported that matrix interferences could affect the nebulizer performance; therefore, optimal instrumental modulation conditions are affected by sample purity . However, this problem can be minimized by the separation of the analyte from the matrix .…”

Section: Introductionmentioning

confidence: 99%

Combination of Syringe–Solid Phase Extraction with Inductively Coupled Plasma Mass Spectrometry for Efficient Heavy Metals Detection

Habila

ALOthman

El‐Toni

et al. 2016

CLEAN Soil Air Water

View full text Add to dashboard Cite

This work aimed to combine solid phase extraction (SPE) with inductively coupled plasma mass spectrometry for the determination of multi-elements (Pb, Cd, and Zn) simultaneously. This combination allows the purification of the solution by minimizing matrix effects, the separation of the analytes and a fast determination of multiple elements (Pb, Cd, and Zn) in seconds. A syringe-solid phase extraction (SYRINGE-SPE) method was developed based on adsorption/desorption of metals onto amino-functionalized hollow core mesoporous shell silica spheres (NH 2 -HCMSSs). The separation of NH 2 -HCMSSs from aqueous phase was assessed by capping the syringe with 0.2-mm filter. The results showed that the quantitative recovery of analytes was obtained at pH 6 by elution with 3 M HNO 3 . The developed method is applicable in the presence of different coexisting ions. The limit of detection was 0.021, 0.004, and 0.007 mg L À1 for Pb(II), Cd(II), and Zn(II) ions, respectively, whereas the limit of detection of the instrument without combination with the SYRINGE-SPE was 0.699, 0.123, and 0.24 mg L À1 for Pb(II), Cd(II), and Zn(II) ions, respectively. The relative standard deviations were 7.4, 6.2, and 5.4% for Pb(II), Cd(II), and Zn(II), respectively. The method was validated using corn bran (8433) certified reference material. The method was successfully applied for the determination of Pb(II), Cd(II), and Zn(II) in bottled water, tap water, beet, radish, carrot, potato, sweet potato, and turnip samples.Abbreviations: AAS, atomic absorption spectrometry; EDS, energydispersive X-ray spectroscopy; FTIR, Fourier transform infrared; ICP-MS, inductively coupled plasma mass spectrometry; LOD, limit of detection; LOQ, limit of quantification; NH 2 -HCMSS, amino-functionalized hollow core mesoporous shell silica sphere; SEM, scanning electron microscopy; SPE, solid-phase extraction; SYRINGE-SPE, syringe-solid phase extraction; TGA, thermal gravimetric analysis 720

show abstract

“…Determination of these elements requires sufficiently sensitive techniques for detection. In the literature, there are many techniques including flame atomic absorption spectrometry (FAAS) [8,11], electrothermal atomic absorption spectrometry (ETAAS) [12,13] inductively coupled plasma optical emission (ICP-OES) [14][15][16][17][18][19][20][21], mass spectrometry (ICP-MS) [22][23][24], X-ray and total reflection X-ray fluorescence techniques (TXRF), atomic fluorescence spectrometry (AFS), microwave-induced plasma source (MIP-OES and MIP-MS), laser-induced breakdown spectroscopy (LIBS), laserexcited atomic fluorescence spectrometry (LEAFS), and glow discharge mass spectrometry (GD-MS) [25,26].…”

Section: Introductionmentioning

confidence: 99%

“…Modern environmental science maintains an interest in methods, which ensure the following important characteristics: (a) multielement analysis of a wide variety of environmental sample types; (b) it must be able to detect large number of elements at threshold concentration levels for a different type of samples. Among the modern instrumental methods for determination of trace elements, inductively coupled plasma optical emission spectrometry (ICP-OES) is very powerful [14][15][16][17][18][19][20][21].…”

Section: Introductionmentioning

confidence: 99%

“…An optimization of the analytical results in inductively coupled plasma with respect to the elimination of nonspectral matrix effects can be achieved by modifying the different operating parameters. Summarizing the investigation on nonspectral matrix effects in the presence of different matrices, the following conclusions can be drawn [16,17,[38][39][40][41][42][43]:…”

Section: Introductionmentioning

confidence: 99%

See 1 more Smart Citation

Possibilities of High Resolution Inductively Coupled Plasma Optical Emission Spectrometry in the Determination of Trace Elements in Environmental Materials

Velitchkova

Veleva

Velichkov

et al. 2013

Journal of Spectroscopy

View full text Add to dashboard Cite

This paper presents new quantitative data for the spectral interferences obtained by high resolution 40.68 MHz radial viewing inductively coupled plasma optical emission spectrometry (HR-ICP-OES) in the determination of Zn, Cd, Sb, Cu, Mn, Pb, Sn, Cr, U, and Ba in environmental materials in the presence of a complex matrix, containing Al, Ca, Fe, Mg, and Ti. The -concept for quantification of spectral interferences was used. The optimum line selection for trace analysis of a variety of multicomponent matrices requires the choice of prominent lines, which are free or negligibly influenced by line interference problems. The versatility of -concept as basic methodology was experimentally demonstrated in the determination of trace of elements in soil and drinking water. The detection limits are lower in comparison with corresponding threshold concentration levels for soil and drinking water in accordance with environmental regulations. This paper shows the possibilities of present day ICP-OES equipment in the direct determination of trace elements (without preconcentration of impurities) in environmental samples.

show abstract

Trace Element Determination by ICP‐AES and ICP‐MS: Developments and Applications Reported During 2006 and 2007

Cited by 17 publications

References 70 publications

GGR Biennial Review: Atomic Absorption, Inductively Coupled Plasma‐Atomic Emission Spectrometry, Neutron Activation Analysis and X‐Ray Fluorescence Spectrometry Review for 2008–2009

GGR Biennial Review: Atomic Absorption, Inductively Coupled Plasma‐Atomic Emission Spectrometry, Neutron Activation Analysis and X‐Ray Fluorescence Spectrometry Review for 2008–2009

Combination of Syringe–Solid Phase Extraction with Inductively Coupled Plasma Mass Spectrometry for Efficient Heavy Metals Detection

Possibilities of High Resolution Inductively Coupled Plasma Optical Emission Spectrometry in the Determination of Trace Elements in Environmental Materials

Contact Info

Product

Resources

About