Topical Mosquito Repellents X: 2-Oxazolidones

Skinner, W. A.; Crawford, H. T.; Skidmore, D.; Maibach, Howard I.

doi:10.1002/jps.2600660434

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-(Chloromethyl)pyrrolidin-2-one 241

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“…This was prepared by the reaction of thionyl chloride with 1-(hydroxymethyl)pyrrolidin-2-one, following the published procedure, 24 bp 78-80 ЊC/0.05 mmHg (lit., 24 25 This was prepared in a similar way 25…”

Section: -(Chloromethyl)pyrrolidin-2-one 24mentioning

confidence: 99%

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Deoxygenation of tertiary and secondary alcohols ROH by thiol-catalysed radical-chain redox decomposition of derivatives ROCH2X to give RH and XCHO

Dang

Roberts

2002

J. Chem. Soc., Perkin Trans. 1

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Section: -(Chloromethyl)pyrrolidin-2-one 24mentioning

confidence: 99%

“…Oil (yield 89%); δ H 1.18 (3 H, s, Me), 1 25. 1.70 (22 H, m, CH 2 ), 3.36 (3 H, s, OMe), 4.71 (2H, s, OCH 2 O); δ C 19.7, 22.1, 22.6, 25.1, 26.1, 26.5, 34.1, 55.1, 79.3, 90.6 (Found: C, 74.5; H, 12.3.…”

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confidence: 99%