Biology of the Integument 1986
DOI: 10.1007/978-3-662-00989-5_28
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Cited by 4 publications
(12 citation statements)
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“…Thus, HTMU (6), HMMU (7), and HDmPyMU (8), the HONM-based uronium salts, were prepared and tested for peptide synthesis and compared with other uronium/aminium (9)(10)(11)(12)(13)(14) salts currently used in our lab and elsewhere ( Figure 2). HTMU (6) is the tetramethyl derivative and forms part of the group of original Knorr reagents [7] such as N-[(1Hbenzotriazol-1-yl)-(dimethylamino)methylene]-N-methylmethanaminium hexafluorophosphate N-oxide (HBTU, 9), [12] N-[(dimethylamino)-1H-1,2,3-triazolo(4,5-b)pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate N-oxide (HATU, 10), [3,13] and O-[cyano(ethoxycarbonyl)methylidene]amino-1,1,3,3-tetramethyluronium hexafluorophosphate (HOTU, 11).…”
Section: Resultsmentioning
confidence: 99%
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“…Thus, HTMU (6), HMMU (7), and HDmPyMU (8), the HONM-based uronium salts, were prepared and tested for peptide synthesis and compared with other uronium/aminium (9)(10)(11)(12)(13)(14) salts currently used in our lab and elsewhere ( Figure 2). HTMU (6) is the tetramethyl derivative and forms part of the group of original Knorr reagents [7] such as N-[(1Hbenzotriazol-1-yl)-(dimethylamino)methylene]-N-methylmethanaminium hexafluorophosphate N-oxide (HBTU, 9), [12] N-[(dimethylamino)-1H-1,2,3-triazolo(4,5-b)pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate N-oxide (HATU, 10), [3,13] and O-[cyano(ethoxycarbonyl)methylidene]amino-1,1,3,3-tetramethyluronium hexafluorophosphate (HOTU, 11).…”
Section: Resultsmentioning
confidence: 99%
“…HTMU (6) is the tetramethyl derivative and forms part of the group of original Knorr reagents [7] such as N-[(1Hbenzotriazol-1-yl)-(dimethylamino)methylene]-N-methylmethanaminium hexafluorophosphate N-oxide (HBTU, 9), [12] N-[(dimethylamino)-1H-1,2,3-triazolo(4,5-b)pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate N-oxide (HATU, 10), [3,13] and O-[cyano(ethoxycarbonyl)methylidene]amino-1,1,3,3-tetramethyluronium hexafluorophosphate (HOTU, 11). [14] HMMU (7) incorporates a morpholino group as a hydrogen-bond acceptor in the uronium part, similarly to 1-{[1-(cyano-2-ethoxy-2-oxoethylideneaminooxy)dimethylaminomorpholinomethylene]}methanaminium hexafluorophosphate (COMU, 12), 1-[(dimethylamino)(morpholino)methylene]-1H-benzotriazolium hexafluorophosphate 3-oxide (HDMB, 13), and 1-[(dimethylamino)(morpholino)methylene]-1H- [1,3]triazolo-[4,5-b]pyridinium hexafluorophosphate 3-oxide (HDMA, 14). These reagents have shown superiority to those described previously, as the oxygen in the uronium/ iminium skeleton confers the reagent greater solubility, enhances coupling yields and decreases racemization, thereby allowing the use of only 1 equiv.…”
Section: Resultsmentioning
confidence: 99%
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“…Formation and degradation of radioactive moniliformin 3 from [2-I4C]acetate[67]. dpm = disintegrations per minute Giberella fujikuroi.…”
mentioning
confidence: 99%