2007
DOI: 10.1007/s10973-005-7471-4
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Thermoanalytical study of fluoxetine hydrochloride

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Cited by 24 publications
(16 citation statements)
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“…Approximately 5 mg of samples were placed in platinum pans and heated for 5, 10, 15, 20 and 25 • C min −1 at the temperature range of 25-800 • C under dynamic synthetic air atmosphere with a flow rate of 50 mL min −1 . The kinetics parameters were determined through the Ozawa method using Shimadzu TASYS software [24,25].…”
Section: Kinetics Analysismentioning
confidence: 99%
“…Approximately 5 mg of samples were placed in platinum pans and heated for 5, 10, 15, 20 and 25 • C min −1 at the temperature range of 25-800 • C under dynamic synthetic air atmosphere with a flow rate of 50 mL min −1 . The kinetics parameters were determined through the Ozawa method using Shimadzu TASYS software [24,25].…”
Section: Kinetics Analysismentioning
confidence: 99%
“…The analysis was carried out using 2 mg of the sample at a heating rate of 2°C/min in the temperature range from 25 to 180°C in a nitrogen atmosphere with a flow rate of 50 ml/min. The analysis was carried out in triplicate [23,24]. The DSC equipment was preliminarily calibrated with a standard reference of indium.…”
Section: Experimental Partmentioning
confidence: 99%
“…The purity determination of substances using differencial scanning calorimetry has been reported in several studies [23,24]. The purity is calculated based on the assumption that impurities will depress the melting point of pure materials.…”
mentioning
confidence: 99%
“…Para que uma técnica térmica seja considerada termoanalítica é necessário, segundo a definição, envolver a medição de uma propriedade física, expressa direta ou indiretamente em função da temperatura, e executada sob um programa controlado desta variável (SILVA et al, 2007).…”
Section: Análise Térmicaunclassified
“…A calorimetria exploratória diferencial (DSC) e a termogravimetria (TG) são as técnicas termoanalíticas mais difundidas e empregadas no desenvolvimento de diferentes estudos sendo aplicadas a uma grande variedade de materiais farmacêuticos (SILVA et al, 2007 …”
Section: Análise Térmicaunclassified