Thermal evolution in air and argon of nanocrystalline MoS2 synthesized under hydrothermal conditions

Synthesis of hierarchical MoS2 and its electrochemical performance as an anode material for lithium-ion batteries

“…1 shows the XRD patterns of the MoS 2 calcined at 450 C for 5 h in the N 2 atmosphere. Thermal evolution of the hydrothermally synthesized MoS 2 has been systematically investigated by Bokhimi et al, 27 which demonstrates that postannealing is helpful to remove the hydroxyls on the particle surface and improve the crystallization. XRD and TG results also prove the improvement of crystallization (Fig.…”

Synthetic approaches to the molybdenum sulfide materials

“…Bokhimi et al [148] studied thermal evolution in air and argon of nanocrystalline MoS 2 synthesized under hydrothermal conditions. Nanocrystalline molybdenum sulfide was synthesized between 150 and 225 C under hydrothermal conditions starting from ammonium heptamolybdate and thiourea.…”

A new synthesis approach of hierarchical MoS2 nanoflakes toward hydrogen evolution in both acidic and alkaline media

“…[11][12][13] Meanwhile, the traditional thermal synthesis procedures suffer from toxic chemicals, high-temperature, high-pressure, and/or long reaction time. [14][15][16] For the conventional thermal techniques using the reaction vessel as an intermediary, good conduction of blackbody radiation is required for heat transfer from the heating mantle to the solution in order to drive the reaction. This kind of heating will cause sharp thermal gradients in the bulk solution, resulting in nonuniform and inefficient reaction conditions, which will further hinder the uniform nucleation and growth of materials.…”